{(2S,4S,5R,6R)-5-Azido-4-benzyloxy-6-[(1R,2S,3R,4R,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-(4-methoxy-benzyloxy)-cyclohexyloxy]-tetrahydro-pyran-2-yl}-methanol

Base Information

Chemical Name:{(2S,4S,5R,6R)-5-Azido-4-benzyloxy-6-[(1R,2S,3R,4R,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-(4-methoxy-benzyloxy)-cyclohexyloxy]-tetrahydro-pyran-2-yl}-methanol
CAS No.:714957-24-1
Molecular Formula:C₅₅H₅₉N₃O₁₀
Molecular Weight:922.088
Hs Code.:

{(2S,4S,5R,6R)-5-Azido-4-benzyloxy-6-[(1R,2S,3R,4R,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-(4-methoxy-benzyloxy)-cyclohexyloxy]-tetrahydro-pyran-2-yl}-methanol

Synonyms:{(2S,4S,5R,6R)-5-Azido-4-benzyloxy-6-[(1R,2S,3R,4R,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-(4-methoxy-benzyloxy)-cyclohexyloxy]-tetrahydro-pyran-2-yl}-methanol

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Chemical Property of {(2S,4S,5R,6R)-5-Azido-4-benzyloxy-6-[(1R,2S,3R,4R,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-(4-methoxy-benzyloxy)-cyclohexyloxy]-tetrahydro-pyran-2-yl}-methanol

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Technology Process of {(2S,4S,5R,6R)-5-Azido-4-benzyloxy-6-[(1R,2S,3R,4R,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-(4-methoxy-benzyloxy)-cyclohexyloxy]-tetrahydro-pyran-2-yl}-methanol

There total 10 articles about {(2S,4S,5R,6R)-5-Azido-4-benzyloxy-6-[(1R,2S,3R,4R,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-(4-methoxy-benzyloxy)-cyclohexyloxy]-tetrahydro-pyran-2-yl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 324739-94-8
1D-6-O-(6-O-acetyl-2-azido-3-O-benzyl-2,4-dideoxy-α-D-xylo-hexopyranosyl)-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-myo-inositol

: 714957-24-1
{(2S,4S,5R,6R)-5-Azido-4-benzyloxy-6-[(1R,2S,3R,4R,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-(4-methoxy-benzyloxy)-cyclohexyloxy]-tetrahydro-pyran-2-yl}-methanol

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; at 20 ℃; for 1.5h;
DOI:10.1016/j.carres.2004.02.026

Reference yield:

: 129261-63-8
(+)-1D-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-myo-inositol

: 714957-24-1
{(2S,4S,5R,6R)-5-Azido-4-benzyloxy-6-[(1R,2S,3R,4R,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-(4-methoxy-benzyloxy)-cyclohexyloxy]-tetrahydro-pyran-2-yl}-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / 1,1,3,3-tetramethylurea; AgClO₄ / Cp₂ZrCl₂ / diethyl ether

2: 97 percent / MeONa / methanol; tetrahydrofuran / 1.5 h / 20 °C

With sodium methylate; silver perchlorate; tetramethylurea; zirconocene dichloride; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1016/j.carres.2004.02.026

Reference yield:

: 55682-57-0
1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

: 714957-24-1
{(2S,4S,5R,6R)-5-Azido-4-benzyloxy-6-[(1R,2S,3R,4R,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-(4-methoxy-benzyloxy)-cyclohexyloxy]-tetrahydro-pyran-2-yl}-methanol

Guidance literature:: Multi-step reaction with 7 steps

1: 79 percent / toluene / 2.5 h / Heating

2: 55 percent / Bu₃SnH; AIBN / benzene / 0.5 h / Heating

3: 74 percent / TFA / 20 °C

4: 81 percent / Me₂NH / acetonitrile; tetrahydrofuran / 6 h / 20 °C

5: DAST / 1,2-dichloro-ethane / -30 °C

6: 35 percent / 1,1,3,3-tetramethylurea; AgClO₄ / Cp₂ZrCl₂ / diethyl ether

7: 97 percent / MeONa / methanol; tetrahydrofuran / 1.5 h / 20 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium methylate; silver perchlorate; dimethyl amine; 4,4'-diaminostilbene-2,2'-disulfonic acid; trifluoroacetic acid; tetramethylurea; zirconocene dichloride; In tetrahydrofuran; methanol; diethyl ether; 1,2-dichloro-ethane; toluene; acetonitrile; benzene;
DOI:10.1016/j.carres.2004.02.026