1D-6-O-(2-azido-3,6-di-O-benzyl-2,4-dideoxy-α-D-xylo-hexopyranosyl)-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-myo-inositol

Base Information

Chemical Name:1D-6-O-(2-azido-3,6-di-O-benzyl-2,4-dideoxy-α-D-xylo-hexopyranosyl)-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-myo-inositol
CAS No.:714957-25-2
Molecular Formula:C₆₂H₆₅N₃O₁₀
Molecular Weight:1012.21
Hs Code.:

Synonyms:1D-6-O-(2-azido-3,6-di-O-benzyl-2,4-dideoxy-α-D-xylo-hexopyranosyl)-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1D-6-O-(2-azido-3,6-di-O-benzyl-2,4-dideoxy-α-D-xylo-hexopyranosyl)-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-myo-inositol

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Technology Process of 1D-6-O-(2-azido-3,6-di-O-benzyl-2,4-dideoxy-α-D-xylo-hexopyranosyl)-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-myo-inositol

There total 10 articles about 1D-6-O-(2-azido-3,6-di-O-benzyl-2,4-dideoxy-α-D-xylo-hexopyranosyl)-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 100-39-0
benzyl bromide

: 714957-24-1
{(2S,4S,5R,6R)-5-Azido-4-benzyloxy-6-[(1R,2S,3R,4R,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-(4-methoxy-benzyloxy)-cyclohexyloxy]-tetrahydro-pyran-2-yl}-methanol

: 714957-25-2
1D-6-O-(2-azido-3,6-di-O-benzyl-2,4-dideoxy-α-D-xylo-hexopyranosyl)-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-myo-inositol

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 2h;
DOI:10.1016/j.carres.2004.02.026

Reference yield:

: 129261-63-8
(+)-1D-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-myo-inositol

: 714957-25-2
1D-6-O-(2-azido-3,6-di-O-benzyl-2,4-dideoxy-α-D-xylo-hexopyranosyl)-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent / 1,1,3,3-tetramethylurea; AgClO₄ / Cp₂ZrCl₂ / diethyl ether

2: 97 percent / MeONa / methanol; tetrahydrofuran / 1.5 h / 20 °C

3: 67 percent / NaH / dimethylformamide / 2 h / 0 °C

With sodium methylate; silver perchlorate; sodium hydride; tetramethylurea; zirconocene dichloride; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2004.02.026

Reference yield:

: 324739-93-7
6-O-acetyl-2-azido-3-O-benzyl-2,4-dideoxy-D-xylo-hexopyranosyl fluoride

: 714957-25-2
1D-6-O-(2-azido-3,6-di-O-benzyl-2,4-dideoxy-α-D-xylo-hexopyranosyl)-2,3,4,5-tetra-O-benzyl-1-O-(4-methoxybenzyl)-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent / 1,1,3,3-tetramethylurea; AgClO₄ / Cp₂ZrCl₂ / diethyl ether

2: 97 percent / MeONa / methanol; tetrahydrofuran / 1.5 h / 20 °C

3: 67 percent / NaH / dimethylformamide / 2 h / 0 °C

With sodium methylate; silver perchlorate; sodium hydride; tetramethylurea; zirconocene dichloride; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2004.02.026