(1R)-cis-1,2,2-trimethyl-3-((S)-1-phenyl-ethylcarbamoyl)-cyclopentanecarboxylic acid ; (d-camphoric acid )-α-(l-α-phenethylamide)

Base Information

Chemical Name:(1R)-cis-1,2,2-trimethyl-3-((S)-1-phenyl-ethylcarbamoyl)-cyclopentanecarboxylic acid ; (d-camphoric acid )-α-(l-α-phenethylamide)
CAS No.:313343-45-2
Molecular Formula:C₁₈H₂₅NO₃
Molecular Weight:303.401
Hs Code.:

(1<i>R</i>)-<i>cis</i>-1,2,2-trimethyl-3-((<i>S</i>)-1-phenyl-ethylcarbamoyl)-cyclopentanecarboxylic acid ; (d-camphoric acid )-α-(l-α-phenethylamide)

Synonyms:(1R)-cis-1,2,2-trimethyl-3-((S)-1-phenyl-ethylcarbamoyl)-cyclopentanecarboxylic acid ; (d-camphoric acid )-α-(l-α-phenethylamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R)-cis-1,2,2-trimethyl-3-((S)-1-phenyl-ethylcarbamoyl)-cyclopentanecarboxylic acid ; (d-camphoric acid )-α-(l-α-phenethylamide)

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Technology Process of (1R)-cis-1,2,2-trimethyl-3-((S)-1-phenyl-ethylcarbamoyl)-cyclopentanecarboxylic acid ; (d-camphoric acid )-α-(l-α-phenethylamide)

There total 3 articles about (1R)-cis-1,2,2-trimethyl-3-((S)-1-phenyl-ethylcarbamoyl)-cyclopentanecarboxylic acid ; (d-camphoric acid )-α-(l-α-phenethylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 618-36-0
rac-methylbenzylamine

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 313343-45-2
(1R)-cis-1,2,2-trimethyl-3-((S)-1-phenyl-ethylcarbamoyl)-cyclopentanecarboxylic acid ; (d-camphoric acid )-α-(l-α-phenethylamide)

Guidance literature:: With camphoric anhydride; man verseift das entstehende -α- mit siedender 30prozentiger Salzsaeure;

Reference yield:

: 98-86-2
acetophenone

: 313343-45-2
(1R)-cis-1,2,2-trimethyl-3-((S)-1-phenyl-ethylcarbamoyl)-cyclopentanecarboxylic acid ; (d-camphoric acid )-α-(l-α-phenethylamide)

Guidance literature:: Multi-step reaction with 2 steps

1: Verseifen des entstehenden Formylderivates mittels siedender Salzsaeure

2: camphoric acid anhydride / man verseift das entstehende -α- mit siedender 30prozentiger Salzsaeure

With camphoric anhydride;

Reference yield:

: 618-36-0
rac-methylbenzylamine

: 595-29-9
camphoric anhydride

: 313343-45-2
(1R)-cis-1,2,2-trimethyl-3-((S)-1-phenyl-ethylcarbamoyl)-cyclopentanecarboxylic acid ; (d-camphoric acid )-α-(l-α-phenethylamide)

: 78854-42-9
(+)-(1R,3S)-1,2,2-trimethyl-3-<((R)-1-phenylethyl)carbamoyl>cyclopentane-1-carboxylic acid

Guidance literature:: man trennt die beiden Formen durch fraktionierte Krystallisation aus Benzol und Alkohol; das Derivat des d-α-Phenaethylamins ist das weniger loesliche;

upstream raw materials:

rac-methylbenzylamine

camphoric anhydride

acetophenone

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