Technology Process of C23H28ClNO5
There total 3 articles about C23H28ClNO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium on carbon; hydrogen / tetrahydrofuran / 12 h / 23 °C
2.1: dichloro-acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dimethyl sulfoxide; toluene / 6 h / 23 °C / Inert atmosphere
3.1: n-butyllithium; zinc(II) chloride / Inert atmosphere
3.2: Inert atmosphere
With
dichloro-acetic acid; n-butyllithium; palladium on carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc(II) chloride;
In
tetrahydrofuran; dimethyl sulfoxide; toluene;
2.1: Moffatt oxidation;
DOI:10.1021/jo101638r
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dichloro-acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dimethyl sulfoxide; toluene / 6 h / 23 °C / Inert atmosphere
2.1: n-butyllithium; zinc(II) chloride / Inert atmosphere
2.2: Inert atmosphere
With
dichloro-acetic acid; n-butyllithium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc(II) chloride;
In
dimethyl sulfoxide; toluene;
1.1: Moffatt oxidation;
DOI:10.1021/jo101638r
- Guidance literature:
-
tributyl(cyclohex-2-en-1-yl)stannane;
With
n-butyllithium; zinc(II) chloride;
Inert atmosphere;
C17H18ClNO5;
In
tetrahydrofuran;
optical yield given as %de;
Inert atmosphere;
DOI:10.1021/jo101638r
