ethyl 4-nitrophenyl {3-[4-(aminomethyl)-1H-1,2,3-triazol-1-yl]-propyl}phosphonate

Base Information

Chemical Name:ethyl 4-nitrophenyl {3-[4-(aminomethyl)-1H-1,2,3-triazol-1-yl]-propyl}phosphonate
CAS No.:1237747-46-4
Molecular Formula:C₁₄H₂₀N₅O₅P
Molecular Weight:369.317
Hs Code.:

Synonyms:ethyl 4-nitrophenyl {3-[4-(aminomethyl)-1H-1,2,3-triazol-1-yl]-propyl}phosphonate

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Chemical Property of ethyl 4-nitrophenyl {3-[4-(aminomethyl)-1H-1,2,3-triazol-1-yl]-propyl}phosphonate

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Technology Process of ethyl 4-nitrophenyl {3-[4-(aminomethyl)-1H-1,2,3-triazol-1-yl]-propyl}phosphonate

There total 1 articles about ethyl 4-nitrophenyl {3-[4-(aminomethyl)-1H-1,2,3-triazol-1-yl]-propyl}phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1237747-44-2
ethyl 4-nitrophenyl (3-azidopropyl)phosphonate

: 2450-71-7
Propargylamine

: 1237747-46-4
ethyl 4-nitrophenyl {3-[4-(aminomethyl)-1H-1,2,3-triazol-1-yl]-propyl}phosphonate

Guidance literature:: With 2-[(dimethylamino)methyl]benzenethiolato-copper(I); In dichloromethane; Inert atmosphere;
DOI:10.1002/ejic.200900980

Reference yield: 88.0%

: 1237747-46-4
ethyl 4-nitrophenyl {3-[4-(aminomethyl)-1H-1,2,3-triazol-1-yl]-propyl}phosphonate

: 1237837-05-6
[4-carboxy-2,6-bis(pyridin-2-yl)phenyl]platinum(II) chloride

: 1237837-09-0
O₂NC₆H₄OP(O)(OC₂H₅)(CH₂)3C₂HN₃CH₂NHC(O)C₆H₂(C₅H₄N)2PtCl

Guidance literature:: With N,N-diisopropylethylamine; benzotriazole-1-yloxytris(dimethylamino)phosphoniu; In N,N-dimethyl-formamide; Pt-compd. and DMF added to phosphonate-compd. in DMF, cooled to 0°C, N,N-diisopropylethylamine and benzotriazole-1-yloxytris(dimethylamino)phosphonium hexafluorophosphate added, stirred overnight; all volatiles evaporated in vac., dissolved in CH2Cl2, washed with 1 M K2CO3, brine and H2O, dried with Na2SO4, filtered through Celite, all volatiles evaporated in vac.;
DOI:10.1002/ejic.200900980