2-acetoxybenzyl-2,2'-(4',5'-diphenyl-1',3'-dithiolyl)-4,5-diphenyl-1,3-dithiole

Base Information

Chemical Name:2-acetoxybenzyl-2,2'-(4',5'-diphenyl-1',3'-dithiolyl)-4,5-diphenyl-1,3-dithiole
CAS No.:76113-15-0
Molecular Formula:C₃₉H₃₀O₂S₄
Molecular Weight:658.93
Hs Code.:

Synonyms:2-acetoxybenzyl-2,2'-(4',5'-diphenyl-1',3'-dithiolyl)-4,5-diphenyl-1,3-dithiole

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Chemical Property of 2-acetoxybenzyl-2,2'-(4',5'-diphenyl-1',3'-dithiolyl)-4,5-diphenyl-1,3-dithiole

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Technology Process of 2-acetoxybenzyl-2,2'-(4',5'-diphenyl-1',3'-dithiolyl)-4,5-diphenyl-1,3-dithiole

There total 5 articles about 2-acetoxybenzyl-2,2'-(4',5'-diphenyl-1',3'-dithiolyl)-4,5-diphenyl-1,3-dithiole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 76113-14-9
2-hydroxybenzyl-2,2'-(4',5'-diphenyl-1',3'-dithiolyl)-4,5-diphenyl-1,3-dithiole

: 75-36-5
acetyl chloride

: 76113-15-0
2-acetoxybenzyl-2,2'-(4',5'-diphenyl-1',3'-dithiolyl)-4,5-diphenyl-1,3-dithiole

Guidance literature:: With pyridine; at 60 ℃;

Reference yield:

: 100-52-7
benzaldehyde

: 76113-15-0
2-acetoxybenzyl-2,2'-(4',5'-diphenyl-1',3'-dithiolyl)-4,5-diphenyl-1,3-dithiole

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / CCl₃COOH / benzene / 0.25 h / Heating

2: 100 percent / NaBH₄ / 1,2-dimethoxy-ethane / 0.5 h / Ambient temperature

3: 100 percent / pyridine / 60 °C

With pyridine; sodium tetrahydroborate; trichloroacetic acid; In 1,2-dimethoxyethane; benzene;

Reference yield:

: 24395-74-2
2-methoxy-4,5-diphenyl-1,3-dithiole

: 76113-15-0
2-acetoxybenzyl-2,2'-(4',5'-diphenyl-1',3'-dithiolyl)-4,5-diphenyl-1,3-dithiole

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / CCl₃COOH / benzene / 0.25 h / Heating

2: 100 percent / NaBH₄ / 1,2-dimethoxy-ethane / 0.5 h / Ambient temperature

3: 100 percent / pyridine / 60 °C

With pyridine; sodium tetrahydroborate; trichloroacetic acid; In 1,2-dimethoxyethane; benzene;