phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1→6)-2,3,4-tetra-O-benzoyl-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1→6)-2,3,4-tetra-O-benzoyl-β-D-glucopyranoside
CAS No.:216006-43-8
Molecular Formula:C₆₇H₅₄O₁₇S
Molecular Weight:1163.22
Hs Code.:

Synonyms:phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1→6)-2,3,4-tetra-O-benzoyl-β-D-glucopyranoside

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Chemical Property of phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1→6)-2,3,4-tetra-O-benzoyl-β-D-glucopyranoside

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Technology Process of phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1→6)-2,3,4-tetra-O-benzoyl-β-D-glucopyranoside

There total 10 articles about phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1→6)-2,3,4-tetra-O-benzoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1439813-22-5
phenyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→6)-1-thio-β-D-glucopyranoside

: 98-88-4
benzoyl chloride

: 216006-43-8
phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1→6)-2,3,4-tetra-O-benzoyl-β-D-glucopyranoside

Guidance literature:: With pyridine; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201300026

Reference yield: 78.0%

: 105376-04-3,138661-53-7,113214-71-4
ethyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

: phenyl 2,3,4-tri-O-benzoyl-1-thio-β-D-glucopyranoside

: 216006-43-8
phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1→6)-2,3,4-tetra-O-benzoyl-β-D-glucopyranoside

Guidance literature:: ethyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside; phenyl 2,3,4-tri-O-benzoyl-1-thio-β-D-glucopyranoside; With 2-((trifluoromethyl)thio)benzo[d]isothiazol-3(2H)-one 1,1-dioxide; In dichloromethane; at 20 ℃; for 0.25h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 0.666667h; chemoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1039/d0ob01606c

Reference yield: 66.0%

: phenyl 2,3,4-tri-O-benzoyl-1-thio-β-D-glucopyranoside

: 183367-63-7
1-p-methylphenyltelluro-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside

: 216006-43-8
phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1→6)-2,3,4-tetra-O-benzoyl-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -23 - 20 ℃;
DOI:10.1016/S0040-4039(98)01753-5