C₁₇H₂₃NO₄

Base Information

• Chemical Name: C₁₇H₂₃NO₄
• CAS No.: 1429302-13-5
• Molecular Formula: C₁₇H₂₃NO₄
• Molecular Weight: 305.374
• Mol file: 1429302-13-5.mol

Synonyms:C₁₇H₂₃NO₄

Chemical Property of C₁₇H₂₃NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₃NO₄

There total 4 articles about C₁₇H₂₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C22H33NO6 (1429302-12-4) → C17H23NO4 (1429302-13-5)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; at 0 ℃; for 0.5h; enantioselective reaction;

DOI:10.1016/j.tetlet.2013.02.059

Reference yield:

(R)-3-hydroxy-N-(4-methoxybenzyl)pyrrolidine-2,5-dione (1312764-95-6) → C17H23NO4 (1429302-13-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: silver(l) oxide / acetonitrile

2.1: magnesium / tetrahydrofuran / 50 °C / Inert atmosphere; Reflux

2.2: 2.5 h / -20 - -10 °C

2.3: 20 °C

3.1: toluene-4-sulfonic acid / dichloromethane / 0.5 h / 0 °C

With toluene-4-sulfonic acid; magnesium; silver(l) oxide; In tetrahydrofuran; dichloromethane; acetonitrile;

DOI:10.1016/j.tetlet.2013.02.059

Reference yield:

4-methoxy-benzylamine (2393-23-9) → C17H23NO4 (1429302-13-5)

Guidance literature:

Multi-step reaction with 4 steps

1.1: m-xylene / Reflux

2.1: silver(l) oxide / acetonitrile

3.1: magnesium / tetrahydrofuran / 50 °C / Inert atmosphere; Reflux

3.2: 2.5 h / -20 - -10 °C

3.3: 20 °C

4.1: toluene-4-sulfonic acid / dichloromethane / 0.5 h / 0 °C

With toluene-4-sulfonic acid; magnesium; silver(l) oxide; In tetrahydrofuran; dichloromethane; m-xylene; acetonitrile;

DOI:10.1016/j.tetlet.2013.02.059

upstream raw materials:

(R)-3-hydroxy-N-(4-methoxybenzyl)pyrrolidine-2,5-dione

C₁₃H₁₅NO₄

C₂₂H₃₃NO₆

4-methoxy-benzylamine