C₁₈H₂₈O₃

Base Information

Chemical Name:C₁₈H₂₈O₃
CAS No.:1228294-02-7
Molecular Formula:C₁₈H₂₈O₃
Molecular Weight:292.419
Hs Code.:

C<sub>18</sub>H<sub>28</sub>O<sub>3</sub>

Synonyms:C₁₈H₂₈O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₈O₃

Chemical Property:

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Technology Process of C₁₈H₂₈O₃

There total 4 articles about C₁₈H₂₈O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1204754-02-8
C₁₄H₂₀O₃

: 115-11-7,15220-85-6
isobutene

: 1228294-02-7
C₁₈H₂₈O₃

Guidance literature:: isobutene; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; at -78 - 20 ℃; Inert atmosphere;

With (-)-B-methoxydiisopinocampheylborane; In diethyl ether; hexane; at -78 - 20 ℃; for 2h; Inert atmosphere;

C₁₄H₂₀O₃; optical yield given as %de; Further stages;
DOI:10.1002/anie.201000624

Reference yield:

: 18292-38-1
2-methallyltrimethylsilane

: 1204754-02-8
C₁₄H₂₀O₃

: 1228294-02-7
C₁₈H₂₈O₃

: C₁₈H₂₈O₃

Guidance literature:: With magnesium bromide diethyl etherate; In dichloromethane; at 0 ℃; Overall yield = 73 %; Overall yield = 1.77 g;
DOI:10.1002/chem.201300664

Reference yield:

: C₉H₁₈OS₂

: 1228294-02-7
C₁₈H₂₈O₃

: C₁₈H₂₈O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / 20 °C

1.2: 4.5 h / 20 °C

2.1: sodium hydrogencarbonate / acetonitrile; water / 20 °C

3.1: magnesium bromide diethyl etherate / dichloromethane / 0 °C

With potassium tert-butylate; magnesium bromide diethyl etherate; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1002/chem.201300664