C₃₅H₄₂O₁₃

Base Information

Chemical Name:C₃₅H₄₂O₁₃
CAS No.:266676-42-0
Molecular Formula:C₃₅H₄₂O₁₃
Molecular Weight:670.711
Hs Code.:

C<sub>35</sub>H<sub>42</sub>O<sub>13</sub>

Synonyms:C₃₅H₄₂O₁₃

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Chemical Property of C₃₅H₄₂O₁₃

Chemical Property:

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Technology Process of C₃₅H₄₂O₁₃

There total 13 articles about C₃₅H₄₂O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 108-30-5
succinic acid anhydride

: 266676-41-9
C₃₁H₃₈O₁₀

: 266676-42-0
C₃₅H₄₂O₁₃

Guidance literature:: With dmap; In N,N-dimethyl-formamide; at 85 ℃; for 48h;
DOI:10.1016/S0960-894X(00)00031-7

Reference yield:

: 11034-45-0
1β,2α,9α,10β-tetrahydroxy-5α-cinnamoyloxytaxa-4(20),11-dien-13-one

: 266676-42-0
C₃₅H₄₂O₁₃

Guidance literature:: Multi-step reaction with 12 steps

1: 73 percent / CuSO₄

2: 92 percent / pyridine / CH₂Cl₂ / 0 °C

3: 65 percent / aq. H₂NOH*HCl; NaOAc / ethanol / Heating

4: 86 percent / aq. OsO₄; NMO / tetrahydrofuran / 20 °C

5: 95 percent / imidazole / dimethylformamide / 20 °C

6: 81 percent / pyridine

7: TBAF / tetrahydrofuran

8: Bu₄N⁺AcO^- / butan-2-one / Heating

9: 71 percent / aq. AcOH / tetrahydrofuran / 40 °C

10: 76 percent / DMAP / 0 - 20 °C

11: 84 percent / tetrahydrofuran / -78 °C

12: 69 percent / DMAP / dimethylformamide / 48 h / 85 °C

With pyridine; 1H-imidazole; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; sodium acetate; tetrabutylammonium acetate; copper(II) sulfate; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; butanone; 1: ketalization / 2: cyclocondensation / 3: Hydrolysis / 4: dihydroxylation / 5: silylation / 6: mesylation / 7: desilylation / 8: Cyclization / 9: deketalization / 10: Acetylation / 11: Addition / 12: Addition;
DOI:10.1016/S0960-894X(00)00031-7

Reference yield:

: 13452-36-3
2,9,10-triacetyl-5-O-cinnamoyltaxicin-I

: 266676-42-0
C₃₅H₄₂O₁₃

Guidance literature:: Multi-step reaction with 13 steps

1: 86 percent / NaOCH₃ / methanol; CH₂Cl₂ / 0 °C

2: 73 percent / CuSO₄

3: 92 percent / pyridine / CH₂Cl₂ / 0 °C

4: 65 percent / aq. H₂NOH*HCl; NaOAc / ethanol / Heating

5: 86 percent / aq. OsO₄; NMO / tetrahydrofuran / 20 °C

6: 95 percent / imidazole / dimethylformamide / 20 °C

7: 81 percent / pyridine

8: TBAF / tetrahydrofuran

9: Bu₄N⁺AcO^- / butan-2-one / Heating

10: 71 percent / aq. AcOH / tetrahydrofuran / 40 °C

11: 76 percent / DMAP / 0 - 20 °C

12: 84 percent / tetrahydrofuran / -78 °C

13: 69 percent / DMAP / dimethylformamide / 48 h / 85 °C

With pyridine; 1H-imidazole; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; sodium methylate; sodium acetate; tetrabutylammonium acetate; copper(II) sulfate; acetic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; butanone; 1: Deacetylation / 2: ketalization / 3: cyclocondensation / 4: Hydrolysis / 5: dihydroxylation / 6: silylation / 7: mesylation / 8: desilylation / 9: Cyclization / 10: deketalization / 11: Acetylation / 12: Addition / 13: Addition;
DOI:10.1016/S0960-894X(00)00031-7