1-(4,5-dimethoxy-2-nitrophenyl)-N,N,N',N'-tetrakispyridin-2-ylmethylethane-1,2-diamine

Base Information

Chemical Name:1-(4,5-dimethoxy-2-nitrophenyl)-N,N,N',N'-tetrakispyridin-2-ylmethylethane-1,2-diamine
CAS No.:1298069-29-0
Molecular Formula:C₃₄H₃₅N₇O₄
Molecular Weight:605.696
Hs Code.:

Synonyms:1-(4,5-dimethoxy-2-nitrophenyl)-N,N,N',N'-tetrakispyridin-2-ylmethylethane-1,2-diamine

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Chemical Property of 1-(4,5-dimethoxy-2-nitrophenyl)-N,N,N',N'-tetrakispyridin-2-ylmethylethane-1,2-diamine

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Technology Process of 1-(4,5-dimethoxy-2-nitrophenyl)-N,N,N',N'-tetrakispyridin-2-ylmethylethane-1,2-diamine

There total 5 articles about 1-(4,5-dimethoxy-2-nitrophenyl)-N,N,N',N'-tetrakispyridin-2-ylmethylethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.4%

: 1297302-53-4
1-(3,4-dimethoxyphenyl)-N,N,N',N'-tetrakispyridin-2-ylmethyl-ethane-1,2-diamine

: 1298069-29-0
1-(4,5-dimethoxy-2-nitrophenyl)-N,N,N',N'-tetrakispyridin-2-ylmethylethane-1,2-diamine

Guidance literature:: With trifluorormethanesulfonic acid; nitric acid; In dichloromethane; at -42 ℃; for 10h;
DOI:10.1002/chem.201001982

Reference yield:

: 1297302-47-6
[2-(bispyridin-2-ylmethylamino)-1-(3,4-dimethoxyphenyl)ethyl]-carbamicacid tert-butyl ester

: 1298069-29-0
1-(4,5-dimethoxy-2-nitrophenyl)-N,N,N',N'-tetrakispyridin-2-ylmethylethane-1,2-diamine

Guidance literature:: Multi-step reaction with 5 steps

1: trifluoroacetic acid / dichloromethane / 24 h / 23 °C

2: ethanol / 1 h / 78 °C

3: sodium tetrahydroborate / ethanol / 24 h / 23 °C

4: sodium tris(acetoxy)borohydride / dichloromethane / 24 h / 23 °C

5: trifluorormethanesulfonic acid; nitric acid / dichloromethane / 10 h / -42 °C

With sodium tetrahydroborate; trifluorormethanesulfonic acid; nitric acid; sodium tris(acetoxy)borohydride; trifluoroacetic acid; In ethanol; dichloromethane;
DOI:10.1002/chem.201001982

Reference yield:

: C₂₈H₃₁N₅O₂

: 1298069-29-0
1-(4,5-dimethoxy-2-nitrophenyl)-N,N,N',N'-tetrakispyridin-2-ylmethylethane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tris(acetoxy)borohydride / dichloromethane / 24 h / 23 °C

2: trifluorormethanesulfonic acid; nitric acid / dichloromethane / 10 h / -42 °C

With trifluorormethanesulfonic acid; nitric acid; sodium tris(acetoxy)borohydride; In dichloromethane;
DOI:10.1002/chem.201001982