1-(3,4-dimethoxyphenyl)-N,N,N',N'-tetrakispyridin-2-ylmethyl-ethane-1,2-diamine

Base Information

Chemical Name:1-(3,4-dimethoxyphenyl)-N,N,N',N'-tetrakispyridin-2-ylmethyl-ethane-1,2-diamine
CAS No.:1297302-53-4
Molecular Formula:C₃₄H₃₆N₆O₂
Molecular Weight:560.699
Hs Code.:

Synonyms:1-(3,4-dimethoxyphenyl)-N,N,N',N'-tetrakispyridin-2-ylmethyl-ethane-1,2-diamine

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Chemical Property of 1-(3,4-dimethoxyphenyl)-N,N,N',N'-tetrakispyridin-2-ylmethyl-ethane-1,2-diamine

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Technology Process of 1-(3,4-dimethoxyphenyl)-N,N,N',N'-tetrakispyridin-2-ylmethyl-ethane-1,2-diamine

There total 4 articles about 1-(3,4-dimethoxyphenyl)-N,N,N',N'-tetrakispyridin-2-ylmethyl-ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: C₂₈H₃₁N₅O₂

: 1297302-53-4
1-(3,4-dimethoxyphenyl)-N,N,N',N'-tetrakispyridin-2-ylmethyl-ethane-1,2-diamine

Guidance literature:: With sodium tris(acetoxy)borohydride; In dichloromethane; at 23 ℃; for 24h;
DOI:10.1002/chem.201001982

Reference yield:

: 1297302-50-1
1-(3,4-dimethoxyphenyl)-N',N'-bispyridin-2-ylmethyl-ethane-1,2-diamine

: 1297302-53-4
1-(3,4-dimethoxyphenyl)-N,N,N',N'-tetrakispyridin-2-ylmethyl-ethane-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 1 h / 78 °C

2: sodium tetrahydroborate / ethanol / 24 h / 23 °C

3: sodium tris(acetoxy)borohydride / dichloromethane / 24 h / 23 °C

With sodium tetrahydroborate; sodium tris(acetoxy)borohydride; In ethanol; dichloromethane;
DOI:10.1002/chem.201001982

Reference yield:

: C₂₈H₂₉N₅O₂

: 1297302-53-4
1-(3,4-dimethoxyphenyl)-N,N,N',N'-tetrakispyridin-2-ylmethyl-ethane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 24 h / 23 °C

2: sodium tris(acetoxy)borohydride / dichloromethane / 24 h / 23 °C

With sodium tetrahydroborate; sodium tris(acetoxy)borohydride; In ethanol; dichloromethane;
DOI:10.1002/chem.201001982