(S)-5-Benzyloxy-1-[(E)-2-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-vinyl]-1-(3-triisopropylsilanyloxy-propyl)-pentylamine

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Chemical Name:(S)-5-Benzyloxy-1-[(E)-2-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-vinyl]-1-(3-triisopropylsilanyloxy-propyl)-pentylamine
CAS No.:920749-76-4
Molecular Formula:C₃₆H₆₅NO₂Si
Molecular Weight:572.003
Hs Code.:

Synonyms:(S)-5-Benzyloxy-1-[(E)-2-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-vinyl]-1-(3-triisopropylsilanyloxy-propyl)-pentylamine

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Chemical Property of (S)-5-Benzyloxy-1-[(E)-2-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-vinyl]-1-(3-triisopropylsilanyloxy-propyl)-pentylamine

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Technology Process of (S)-5-Benzyloxy-1-[(E)-2-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-vinyl]-1-(3-triisopropylsilanyloxy-propyl)-pentylamine

There total 5 articles about (S)-5-Benzyloxy-1-[(E)-2-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-vinyl]-1-(3-triisopropylsilanyloxy-propyl)-pentylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 920750-13-6
[(S)-5-Benzyloxy-1-[(E)-2-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-vinyl]-1-(3-triisopropylsilanyloxy-propyl)-pentyl]-carbamic acid 9H-fluoren-9-ylmethyl ester

: 920749-76-4
(S)-5-Benzyloxy-1-[(E)-2-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-vinyl]-1-(3-triisopropylsilanyloxy-propyl)-pentylamine

Guidance literature:: With piperidine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.jorganchem.2006.07.028

Reference yield:

: {8-Benzyloxy-4-[1-iodo-meth-(Z)-ylidene]-octyloxy}-triisopropyl-silane

: 920749-76-4
(S)-5-Benzyloxy-1-[(E)-2-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-vinyl]-1-(3-triisopropylsilanyloxy-propyl)-pentylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-BuLi / diethyl ether; petroleum ether / 1 h / -78 - 20 °C

1.2: 97 percent / AlMe₃ / diethyl ether; petroleum ether / -78 - 20 °C

2.1: CH₂Cl₂ / 1 h / 0 °C

2.2: potassium carbonate / methanol; H₂O / 0 - 20 °C

2.3: 99 percent / TFAA; triethylamine / CH₂Cl₂ / 0.25 h / 0 °C

3.1: Ti(Ot-Bu)4 / benzene / 3 h / Heating

4.1: 506 mg / piperidine / dimethylformamide; CH₂Cl₂ / 20 °C

With piperidine; titanium(IV) tetrabutoxide; n-butyllithium; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; Petroleum ether; benzene;
DOI:10.1016/j.jorganchem.2006.07.028

Reference yield:

: 920749-68-4
(Z)-(S)-7-Benzyloxy-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-3-(3-triisopropylsilanyloxy-propyl)-hept-2-en-1-ol

: 920749-76-4
(S)-5-Benzyloxy-1-[(E)-2-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-vinyl]-1-(3-triisopropylsilanyloxy-propyl)-pentylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: CH₂Cl₂ / 1 h / 0 °C

1.2: potassium carbonate / methanol; H₂O / 0 - 20 °C

1.3: 99 percent / TFAA; triethylamine / CH₂Cl₂ / 0.25 h / 0 °C

2.1: Ti(Ot-Bu)4 / benzene / 3 h / Heating

3.1: 506 mg / piperidine / dimethylformamide; CH₂Cl₂ / 20 °C

With piperidine; titanium(IV) tetrabutoxide; In dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.jorganchem.2006.07.028