1-chloro-2-pentafluorosulfanylcyclohexane

Base Information

• Chemical Name: 1-chloro-2-pentafluorosulfanylcyclohexane
• CAS No.: 1692-53-1
• Molecular Formula: C₆H₁₀ClF₅S
• Molecular Weight: 244.656
• Mol file: 1692-53-1.mol

Synonyms:1-chloro-2-pentafluorosulfanylcyclohexane

Chemical Property of 1-chloro-2-pentafluorosulfanylcyclohexane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 1-chloro-2-pentafluorosulfanylcyclohexane

There total 2 articles about 1-chloro-2-pentafluorosulfanylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

cyclohexene (110-83-8) → 1-chloro-2-pentafluorosulfanylcyclohexane (1692-53-1)

Guidance literature:

With pentafluorosulfanyl chloride; triethyl borane; In hexane; at -30 - 20 ℃;

DOI:10.1021/ol026483o

Reference yield: 98.0%

3,6-dimethylcyclohex-1-ene (19550-40-4) → 1-chloro-2-pentafluorosulfanylcyclohexane (1692-53-1)

Guidance literature:

With pentafluorosulfanyl chloride; triethyl borane; In hexane; at -30 - 20 ℃;

DOI:10.1016/j.jfluchem.2006.05.003

Reference yield: 71.0%

1-chloro-2-pentafluorosulfanylcyclohexane (1692-53-1) → Cyclohexenyl-schwefelpentafluorid (1536-79-4)

Guidance literature:

With potassium tert-butylate; In diethyl ether; at 20 ℃; for 14h;

DOI:10.1016/j.jfluchem.2003.11.028

upstream raw materials:

cyclohexene

3,6-dimethylcyclohex-1-ene

Downstream raw materials:

Cyclohexenyl-schwefelpentafluorid

pentafluorosulfanylbenzene

C₆H₇Br₂F₅S

Refernces

• 1、 Dolbier Jr., William R.,A?t-Mohand, Samia,Schertz, Tyler D.,Sergeeva, Tatiana A.,Cradlebaugh, Joseph A.,Mitani, Akira,Gard, Gary L.,Winter, Rolf W.,Thrasher, Joseph S.. "A convenient and efficient method for incorporation of pentafluorosulfanyl (SF5) substituents into aliphatic compounds". . p. 1302 - 1310. Retrieved 2008/09/17.