dimethyl 3-[3-(4-benzyloxycarbonylaminophenyl)propionylamino]-3',4-oxydibenzoate

Base Information

Chemical Name:dimethyl 3-[3-(4-benzyloxycarbonylaminophenyl)propionylamino]-3',4-oxydibenzoate
CAS No.:227275-06-1
Molecular Formula:C₃₃H₃₀N₂O₈
Molecular Weight:582.61
Hs Code.:

Synonyms:dimethyl 3-[3-(4-benzyloxycarbonylaminophenyl)propionylamino]-3',4-oxydibenzoate

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Chemical Property of dimethyl 3-[3-(4-benzyloxycarbonylaminophenyl)propionylamino]-3',4-oxydibenzoate

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Technology Process of dimethyl 3-[3-(4-benzyloxycarbonylaminophenyl)propionylamino]-3',4-oxydibenzoate

There total 5 articles about dimethyl 3-[3-(4-benzyloxycarbonylaminophenyl)propionylamino]-3',4-oxydibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.4%

: 227275-21-0
dimethyl 3-amino-3',4-oxydibenzoate

: [4-(2-chlorocarbonyl-ethyl)-phenyl]-carbamic acid benzyl ester

: 227275-06-1
dimethyl 3-[3-(4-benzyloxycarbonylaminophenyl)propionylamino]-3',4-oxydibenzoate

Guidance literature:: With triethylamine; In chloroform; at 20 ℃;
DOI:10.1016/S0968-0896(01)00023-2

Reference yield:

: 19438-10-9
methyl 3-hydroxybenzoate

: 227275-06-1
dimethyl 3-[3-(4-benzyloxycarbonylaminophenyl)propionylamino]-3',4-oxydibenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 91.8 percent / K₂CO₃ / dimethylformamide / 6 h / 20 °C

2: H₂ / Pd/C / methanol; dioxane / 1 h / 20 °C / 2280 Torr

3: 72.4 percent / Et₃N / CHCl₃ / 20 °C

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(01)00023-2

Reference yield:

: 329-59-9
4-fluoro-3-nitro-benzoic acid methyl ester

: 227275-06-1
dimethyl 3-[3-(4-benzyloxycarbonylaminophenyl)propionylamino]-3',4-oxydibenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 91.8 percent / K₂CO₃ / dimethylformamide / 6 h / 20 °C

2: H₂ / Pd/C / methanol; dioxane / 1 h / 20 °C / 2280 Torr

3: 72.4 percent / Et₃N / CHCl₃ / 20 °C

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(01)00023-2