{2-bromo-5-[2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-4-fluoro-phenyl}-acetyl-2,2-dimethyl-propionic anhydride

Base Information

Chemical Name:{2-bromo-5-[2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-4-fluoro-phenyl}-acetyl-2,2-dimethyl-propionic anhydride
CAS No.:1232402-61-7
Molecular Formula:C₂₁H₃₂BrFO₅Si
Molecular Weight:491.47
Hs Code.:

Synonyms:{2-bromo-5-[2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-4-fluoro-phenyl}-acetyl-2,2-dimethyl-propionic anhydride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {2-bromo-5-[2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-4-fluoro-phenyl}-acetyl-2,2-dimethyl-propionic anhydride

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Technology Process of {2-bromo-5-[2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-4-fluoro-phenyl}-acetyl-2,2-dimethyl-propionic anhydride

There total 1 articles about {2-bromo-5-[2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-4-fluoro-phenyl}-acetyl-2,2-dimethyl-propionic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1232402-60-6
{2-bromo-5-[2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-4-fluoro-phenyl}-acetic acid

: 3282-30-2
pivaloyl chloride

: 1232402-61-7
{2-bromo-5-[2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-4-fluoro-phenyl}-acetyl-2,2-dimethyl-propionic anhydride

Guidance literature:: With triethylamine; In toluene; at 0 ℃; for 1h;

Reference yield: 50.0%

: 1232402-48-0
(S)-2-(4-fluorophenyl)-2,3-dihydro-1H-pyridin-4-one

: 1232402-61-7
{2-bromo-5-[2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-4-fluoro-phenyl}-acetyl-2,2-dimethyl-propionic anhydride

: 1232402-62-8
1-(2-{2-bromo-5-[2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-4-fluoro-phenyl}-acetyl)-2-(4-fluoro-phenyl)-2,3-dihydro-1H-pyridin-4-one

Guidance literature:: (S)-2-(4-fluorophenyl)-2,3-dihydro-1H-pyridin-4-one; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h;

{2-bromo-5-[2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-4-fluoro-phenyl}-acetyl-2,2-dimethyl-propionic anhydride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1h;