C₄₅H₈₄O₅Si₂

Base Information

Chemical Name:C₄₅H₈₄O₅Si₂
CAS No.:1422039-62-0
Molecular Formula:C₄₅H₈₄O₅Si₂
Molecular Weight:761.33
Hs Code.:

C<sub>45</sub>H<sub>84</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₄₅H₈₄O₅Si₂

Suppliers and Price of C₄₅H₈₄O₅Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₅H₈₄O₅Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₅H₈₄O₅Si₂

There total 15 articles about C₄₅H₈₄O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1112844-75-3
(1S,2R,5S,7R)-7-(5-(benzyloxy)pentyl)-5-(15-hydroxypentadecyl)-6,8-dioxabicyclo[3.2.1]octan-2-ol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1112844-76-4
(1R,2R,5S,7R)-7-(5-(benzyloxy)pentyl)-5-(15-(tert-butyldimethylsilyloxy)pentadecyl)-6,8-dioxabicyclo[3.2.1]octan-2-ol

: 1422039-62-0
C₄₅H₈₄O₅Si₂

Guidance literature:: (1S,2R,5S,7R)-7-(5-(benzyloxy)pentyl)-5-(15-hydroxypentadecyl)-6,8-dioxabicyclo[3.2.1]octan-2-ol; With 1H-imidazole; dmap; In dichloromethane; at 0 ℃; for 0.25h;

tert-butyldimethylsilyl chloride; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/j.tet.2012.12.045

Reference yield:

: 38145-93-6
1,2:3,4-di-O-isopropylidene-D-mannitol

: 1422039-62-0
C₄₅H₈₄O₅Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium periodate / dichloromethane; water / 4 h / 0 - 20 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0 °C

2.2: 0.5 h / 0 °C

3.1: hydrogen / ethanol / 0.5 h / 1034.32 Torr

4.1: toluene-4-sulfonic acid / methanol / 20 h / 0 °C

5.1: di(n-butyl)tin oxide; dmap; triethylamine / dichloromethane / 0.5 h / 20 °C / Cooling with ice

5.2: 4 h / 0 - 20 °C

6.1: potassium carbonate / methanol / 1 h / 0 °C / Inert atmosphere

7.1: n-butyllithium; boron trifluoride diethyl etherate / tetrahydrofuran / 0.75 h / -78 °C

8.1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

9.1: dichloro bis(acetonitrile) palladium(II) / acetonitrile / 20 °C / Inert atmosphere

10.1: dmap; 1H-imidazole / dichloromethane / 0.25 h / 0 °C

10.2: 1 h / 0 °C

With 1H-imidazole; dmap; dichloro bis(acetonitrile) palladium(II); sodium periodate; n-butyllithium; boron trifluoride diethyl etherate; potassium tert-butylate; hydrogen; di(n-butyl)tin oxide; potassium carbonate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile; 2.1: |Wittig Olefination / 2.2: |Wittig Olefination;
DOI:10.1016/j.tet.2012.12.045

Reference yield:

: 62873-30-7
heptadec-16-yn-1-ol

: 1422039-62-0
C₄₅H₈₄O₅Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: dmap; triethylamine / dichloromethane / 0.25 h / 0 °C

1.2: 1 h / 0 °C

2.1: n-butyllithium; boron trifluoride diethyl etherate / tetrahydrofuran / 0.75 h / -78 °C

3.1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

4.1: dichloro bis(acetonitrile) palladium(II) / acetonitrile / 20 °C / Inert atmosphere

5.1: dmap; 1H-imidazole / dichloromethane / 0.25 h / 0 °C

5.2: 1 h / 0 °C

With 1H-imidazole; dmap; dichloro bis(acetonitrile) palladium(II); n-butyllithium; boron trifluoride diethyl etherate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2012.12.045