C₂₇H₄₄O₁₀S

Base Information

Chemical Name:C₂₇H₄₄O₁₀S
CAS No.:943898-25-7
Molecular Formula:C₂₇H₄₄O₁₀S
Molecular Weight:560.706
Hs Code.:

C<sub>27</sub>H<sub>44</sub>O<sub>10</sub>S

Synonyms:C₂₇H₄₄O₁₀S

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Chemical Property of C₂₇H₄₄O₁₀S

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Technology Process of C₂₇H₄₄O₁₀S

There total 6 articles about C₂₇H₄₄O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 943898-27-9
C₂₆H₄₂O₈

: 124-63-0
methanesulfonyl chloride

: 943898-25-7
C₂₇H₄₄O₁₀S

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1021/ol070517g

Reference yield:

: 637002-71-2
(R)-2-(4-Methoxy-phenyl)-4-((S)-1-methyl-allyl)-[1,3]dioxane

: 943898-25-7
C₂₇H₄₄O₁₀S

Guidance literature:: Multi-step reaction with 6 steps

1.1: 70 percent / oxygen; copper(II) acetate monohydrate / PdCl₂ / N,N-dimethyl-acetamide; H₂O / 12 h

2.1: ethyldiisopropylamine; dibutylboron triflate / CH₂Cl₂; diethyl ether / -78 - -50 °C

2.2: CH₂Cl₂; diethyl ether / 6 h / -78 - -50 °C

2.3: 72 percent / aq. H₂O₂ / various solvents / pH 7

3.1: diethyl(methoxy)borane; NaBH₄ / tetrahydrofuran; methanol / -78 °C

3.2: 85 percent / methanol

4.1: 81 percent / ethyldiisopropylamine / CHCl₃ / 12 h / 65 °C

5.1: 78 percent / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

6.1: 91 percent / triethylamine / CH₂Cl₂ / 0 °C

With sodium tetrahydroborate; di-n-butylboryl trifluoromethanesulfonate; diethyl methoxy borane; tetrabutyl ammonium fluoride; oxygen; copper diacetate; triethylamine; N-ethyl-N,N-diisopropylamine; palladium dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl acetamide; water; 1.1: Wacker reaction / 2.2: Evans aldol reaction;
DOI:10.1021/ol070517g

Reference yield:

: 943897-90-3
C₁₅H₂₀O₄

: 943898-25-7
C₂₇H₄₄O₁₀S

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethyldiisopropylamine; dibutylboron triflate / CH₂Cl₂; diethyl ether / -78 - -50 °C

1.2: CH₂Cl₂; diethyl ether / 6 h / -78 - -50 °C

1.3: 72 percent / aq. H₂O₂ / various solvents / pH 7

2.1: diethyl(methoxy)borane; NaBH₄ / tetrahydrofuran; methanol / -78 °C

2.2: 85 percent / methanol

3.1: 81 percent / ethyldiisopropylamine / CHCl₃ / 12 h / 65 °C

4.1: 78 percent / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

5.1: 91 percent / triethylamine / CH₂Cl₂ / 0 °C

With sodium tetrahydroborate; di-n-butylboryl trifluoromethanesulfonate; diethyl methoxy borane; tetrabutyl ammonium fluoride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; 1.2: Evans aldol reaction;
DOI:10.1021/ol070517g