Benzoic acid (1S,2R,3aS,7aS)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2,3,3a,4,7,7a-hexahydro-1H-inden-2-yl ester

Base Information

Chemical Name:Benzoic acid (1S,2R,3aS,7aS)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2,3,3a,4,7,7a-hexahydro-1H-inden-2-yl ester
CAS No.:112168-24-8
Molecular Formula:C₂₃H₃₄O₃Si
Molecular Weight:386.607
Hs Code.:

Synonyms:Benzoic acid (1S,2R,3aS,7aS)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2,3,3a,4,7,7a-hexahydro-1H-inden-2-yl ester

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Chemical Property of Benzoic acid (1S,2R,3aS,7aS)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2,3,3a,4,7,7a-hexahydro-1H-inden-2-yl ester

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Technology Process of Benzoic acid (1S,2R,3aS,7aS)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2,3,3a,4,7,7a-hexahydro-1H-inden-2-yl ester

There total 1 articles about Benzoic acid (1S,2R,3aS,7aS)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2,3,3a,4,7,7a-hexahydro-1H-inden-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-88-4
benzoyl chloride

: 18162-48-6
tert-butyldimethylsilyl chloride

: 112168-19-1
(1S,2R,3aS,7aS)-1-Hydroxymethyl-2,3,3a,4,7,7a-hexahydro-1H-inden-2-ol

: 112168-24-8
Benzoic acid (1S,2R,3aS,7aS)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2,3,3a,4,7,7a-hexahydro-1H-inden-2-yl ester

Guidance literature:: With 1H-imidazole; Yield given. Multistep reaction; 1.) DMF; 2.) pyridine;
DOI:10.1039/c39870000269

Reference yield: 86.0%

: 112168-24-8
Benzoic acid (1S,2R,3aS,7aS)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2,3,3a,4,7,7a-hexahydro-1H-inden-2-yl ester

: 112168-25-9
Benzoic acid (1R,2S,3S,4R)-2-(tert-butyl-dimethyl-silanyloxymethyl)-3,4-bis-carboxymethyl-cyclopentyl ester

Guidance literature:: With potassium permanganate; sodium periodate; sodium carbonate; In 1,4-dioxane; water;
DOI:10.1039/c39870000269

Reference yield:

: 112168-24-8
Benzoic acid (1S,2R,3aS,7aS)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2,3,3a,4,7,7a-hexahydro-1H-inden-2-yl ester

: 112168-26-0
Benzoic acid (1R,2S,3S,4R)-3,4-bis-carboxymethyl-2-hydroxymethyl-cyclopentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / NaIO₄, KMnO₄, Na₂CO₃ / dioxane; H₂O

2: 90 percent / acetic acid; H₂O

With potassium permanganate; sodium periodate; sodium carbonate; In 1,4-dioxane; water; acetic acid;
DOI:10.1039/c39870000269