cyclohex-2-en-1-yl 2,4,6-trimethylbenzoate

Base Information

• Chemical Name: cyclohex-2-en-1-yl 2,4,6-trimethylbenzoate
• CAS No.: 102853-22-5
• Molecular Formula: C₁₆H₂₀O₂
• Molecular Weight: 244.334
• Mol file: 102853-22-5.mol

Synonyms:cyclohex-2-en-1-yl 2,4,6-trimethylbenzoate

Chemical Property of cyclohex-2-en-1-yl 2,4,6-trimethylbenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of cyclohex-2-en-1-yl 2,4,6-trimethylbenzoate

There total 3 articles about cyclohex-2-en-1-yl 2,4,6-trimethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

mesitylenecarboxylic acid (480-63-7) + cyclohexane (110-82-7,25012-93-5) → cyclohex-2-en-1-yl 2,4,6-trimethylbenzoate (102853-22-5)

Guidance literature:

With tert.-butylhydroperoxide; (6,8,15,17-tetramethyldibenzo[b,i][1,4,8,11]tetraazacyclotetradecinato)copper(II); In neat (no solvent); at 80 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1016/j.ica.2019.119190

Reference yield: 95.0%

mesitylenecarboxylic acid (480-63-7) + cyclohexene (110-83-8) → cyclohex-2-en-1-yl 2,4,6-trimethylbenzoate (102853-22-5)

Guidance literature:

With di-tert-butyl peroxide; C₁₁H₂₃N₂⁽¹⁺⁾*Br₄Fe^(1-); In ethyl acetate; at 110 ℃; for 24h;

DOI:10.1016/j.tetlet.2017.05.039

Reference yield:

Cyclohex-2-enol (822-67-3) + mesitylene-2-carboxylic acid chloride (938-18-1) → cyclohex-2-en-1-yl 2,4,6-trimethylbenzoate (102853-22-5)

Guidance literature:

In pyridine; Ambient temperature;

DOI:10.1021/jo00365a006

upstream raw materials:

Cyclohex-2-enol

mesitylene-2-carboxylic acid chloride

mesitylenecarboxylic acid

cyclohexane

Downstream raw materials:

3-methyl-1-cyclohexene

3-n-butylcyclohexene

3-(2-methylpropyl)cyclohexene

3-vinylcyclohexene