n-(4-Methylphenyl)-n-nitrosoacetamide

Base Information

• Chemical Name: n-(4-Methylphenyl)-n-nitrosoacetamide
• CAS No.: 10557-67-2
• Molecular Formula: C9H10N2O2
• Molecular Weight: 178.191
• NSC Number: 95273
• DSSTox Substance ID: DTXSID80294228
• Nikkaji Number: J832.603G
• Wikidata: Q82033409
• Mol file: 10557-67-2.mol

Synonyms:10557-67-2;n-(4-methylphenyl)-n-nitrosoacetamide;NSC95273;DTXSID80294228;NSC-95273

Chemical Property of n-(4-Methylphenyl)-n-nitrosoacetamide

Chemical Property:

• Vapor Pressure: 0.00443mmHg at 25°C
• Boiling Point: 277.8°Cat760mmHg
• Flash Point: 121.8°C
• Density: 1.13g/cm³
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 178.074227566
• Heavy Atom Count: 13
• Complexity: 198

Purity/Quality:

99.5% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)N(C(=O)C)N=O

Technology Process of n-(4-Methylphenyl)-n-nitrosoacetamide

There total 4 articles about n-(4-Methylphenyl)-n-nitrosoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Methylacetanilide (103-89-9) → N-nitroso-p-methyl-acetanilide (10557-67-2)

Guidance literature:

With mixture of gaseous nitrogen oxides; acetic acid;

Reference yield:

→ N-nitroso-p-methyl-acetanilide (10557-67-2)

Guidance literature:

With alkali; und bei -5grad mit Essigsaeureanhydrid schuettelt;

Reference yield:

cis-nitrous acid (7782-77-6) + acetic acid (64-19-7,77671-22-8) + 4-Methylacetanilide (103-89-9) → N-nitroso-p-methyl-acetanilide (10557-67-2)

Guidance literature:

upstream raw materials:

4-Methylacetanilide

cis-nitrous acid

acetic acid

Downstream raw materials:

p-tolyl

4-Methylacetanilide

p-tolyl-[1,4]benzoquinone

4-Methylbiphenyl