1,6-bis-(toluene-4-sulfonyl)-decahydro-[1,6]diazecine

Base Information

Chemical Name:1,6-bis-(toluene-4-sulfonyl)-decahydro-[1,6]diazecine
CAS No.:114721-23-2
Molecular Formula:C₂₂H₃₀N₂O₄S₂
Molecular Weight:450.623
Hs Code.:

Synonyms:1,6-bis-(toluene-4-sulfonyl)-decahydro-[1,6]diazecine

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Chemical Property of 1,6-bis-(toluene-4-sulfonyl)-decahydro-[1,6]diazecine

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Technology Process of 1,6-bis-(toluene-4-sulfonyl)-decahydro-[1,6]diazecine

There total 1 articles about 1,6-bis-(toluene-4-sulfonyl)-decahydro-[1,6]diazecine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-52-1
1,4-dibromo-butane

: 15544-47-5
N,N'-ditosyl-1,4-diaminobutane

: 114721-23-2
1,6-bis-(toluene-4-sulfonyl)-decahydro-[1,6]diazecine

Guidance literature:: With sodium methylate; Yield given. Multistep reaction; 1.) 60 deg C, 2 h; 2.) DMF, 100 deg C, overnight;
DOI:10.1016/S0040-4039(00)78449-8

Reference yield: 68.0%

: 114721-23-2
1,6-bis-(toluene-4-sulfonyl)-decahydro-[1,6]diazecine

: 160096-36-6
1-(Toluene-4-sulfonyl)-[1,6]diazecane

Guidance literature:: With Dowex anion exchange resin; hydrogen bromide; In acetic acid; at 80 ℃; for 16h;
DOI:10.1016/S0040-4039(00)78449-8

Reference yield:

: 114721-23-2
1,6-bis-(toluene-4-sulfonyl)-decahydro-[1,6]diazecine

: 160096-38-8
3-[6-(Toluene-4-sulfonyl)-[1,6]diazecan-1-yl]-propionitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / 1.) 33percent HBr; 2.) Dowex anion exchange resin / acetic acid; various solvent(s) / 16 h / 80 °C

2: 96 percent / toluene / 120 h / Heating

With Dowex anion exchange resin; hydrogen bromide; In acetic acid; toluene;
DOI:10.1016/S0040-4039(00)78449-8