1-(Toluene-4-sulfonyl)-[1,6]diazecane

Base Information

Chemical Name:1-(Toluene-4-sulfonyl)-[1,6]diazecane
CAS No.:160096-36-6
Molecular Formula:C₁₅H₂₄N₂O₂S
Molecular Weight:296.434
Hs Code.:

Synonyms:1-(Toluene-4-sulfonyl)-[1,6]diazecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(Toluene-4-sulfonyl)-[1,6]diazecane

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Technology Process of 1-(Toluene-4-sulfonyl)-[1,6]diazecane

There total 2 articles about 1-(Toluene-4-sulfonyl)-[1,6]diazecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 114721-23-2
1,6-bis-(toluene-4-sulfonyl)-decahydro-[1,6]diazecine

: 160096-36-6
1-(Toluene-4-sulfonyl)-[1,6]diazecane

Guidance literature:: With Dowex anion exchange resin; hydrogen bromide; In acetic acid; at 80 ℃; for 16h;
DOI:10.1016/S0040-4039(00)78449-8

Reference yield:

: 15544-47-5
N,N'-ditosyl-1,4-diaminobutane

: 160096-36-6
1-(Toluene-4-sulfonyl)-[1,6]diazecane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium methoxide / 1.) 60 deg C, 2 h; 2.) DMF, 100 deg C, overnight

2: 68 percent / 1.) 33percent HBr; 2.) Dowex anion exchange resin / acetic acid; various solvent(s) / 16 h / 80 °C

With Dowex anion exchange resin; hydrogen bromide; sodium methylate; In acetic acid;
DOI:10.1016/S0040-4039(00)78449-8