3-(3,4-Bis-phenylacetoxy-phenyl)-2-phenylacetylamino-propionic acid methyl ester

Base Information

Chemical Name:3-(3,4-Bis-phenylacetoxy-phenyl)-2-phenylacetylamino-propionic acid methyl ester
CAS No.:106787-85-3
Molecular Formula:C₃₄H₃₁NO₇
Molecular Weight:565.623
Hs Code.:

Synonyms:3-(3,4-Bis-phenylacetoxy-phenyl)-2-phenylacetylamino-propionic acid methyl ester

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Chemical Property of 3-(3,4-Bis-phenylacetoxy-phenyl)-2-phenylacetylamino-propionic acid methyl ester

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Technology Process of 3-(3,4-Bis-phenylacetoxy-phenyl)-2-phenylacetylamino-propionic acid methyl ester

There total 1 articles about 3-(3,4-Bis-phenylacetoxy-phenyl)-2-phenylacetylamino-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 40611-00-5
DL-3-(3,4-dihydroxyphenyl)alanine methyl ester hydrochloride

: 103-80-0
phenylacetyl chloride

: 106787-85-3
3-(3,4-Bis-phenylacetoxy-phenyl)-2-phenylacetylamino-propionic acid methyl ester

Guidance literature:: With potassium carbonate; In diethyl ether; water; for 2h; Ambient temperature;
DOI:10.1248/cpb.34.1994

Reference yield: 83.0%

: 106787-85-3
3-(3,4-Bis-phenylacetoxy-phenyl)-2-phenylacetylamino-propionic acid methyl ester

: 106787-86-4
3-(3,4-Bis-phenylacetoxy-phenyl)-2-(2-phenyl-thioacetylamino)-propionic acid methyl ester

Guidance literature:: With Lawessons reagent; In 1,2-dimethoxyethane; for 24h; Ambient temperature;
DOI:10.1248/cpb.34.1994

Reference yield:

: 106787-85-3
3-(3,4-Bis-phenylacetoxy-phenyl)-2-phenylacetylamino-propionic acid methyl ester

: 106787-97-7
methyl cis-2-acetyl-6,7-dihydroxy-1-phenylmethyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1: 83 percent / Lawesson's reagent / 1,2-dimethoxy-ethane / 24 h / Ambient temperature

2: 10 percent anhydrous HCl / methanol / 1 h / Ambient temperature

3: 65 percent / 4-nitrobenzyl bromide / acetonitrile / 72 h / Heating

4: 79 percent / H₂ / PtO₂ / methanol / 0.5 h / 760 Torr / Ambient temperature

5: pyridine / 24 h / Ambient temperature

6: 10 percent HCl-CH₃OH / 2 h / Ambient temperature

With Lawessons reagent; pyridine; hydrogenchloride; hydrogen; 1-bromomethyl-4-nitro-benzene; platinum(IV) oxide; In methanol; 1,2-dimethoxyethane; acetonitrile;
DOI:10.1248/cpb.34.1994