2-(2-isopropyl-5-methylphenoxy)ethanethioamide

Base Information

• Chemical Name: 2-(2-isopropyl-5-methylphenoxy)ethanethioamide
• CAS No.: 60988-43-4
• Molecular Formula: C₁₂H₁₇NOS
• Molecular Weight: 223.339
• Mol file: 60988-43-4.mol

Synonyms:2-(2-isopropyl-5-methylphenoxy)ethanethioamide

Chemical Property of 2-(2-isopropyl-5-methylphenoxy)ethanethioamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(2-isopropyl-5-methylphenoxy)ethanethioamide

There total 6 articles about 2-(2-isopropyl-5-methylphenoxy)ethanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

2-(2-isopropyl-5-methylphenoxy)acetamide → 2-(2-isopropyl-5-methylphenoxy)ethanethioamide (60988-43-4)

Guidance literature:

With Lawessons reagent; In toluene; at 150 ℃;

DOI:10.3390/molecules24193435

Reference yield:

thymol (89-83-8) → 2-(2-isopropyl-5-methylphenoxy)ethanethioamide (60988-43-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / acetone / 3 h / 0 - 20 °C

2: Lawessons reagent / toluene / 150 °C

With Lawessons reagent; potassium hydroxide; In acetone; toluene;

DOI:10.3390/molecules24193435

Reference yield:

thymoxyacetaldehyde → 2-(2-isopropyl-5-methylphenoxy)ethanethioamide (60988-43-4)

Guidance literature:

Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride, sodium hydroxide / aq. ethanol; H₂O / Ambient temperature

2: acetic anhydride / Heating

3: hydrogen sulphide gas, triethylamine, pyridine / Ambient temperature

With pyridine; sodium hydroxide; hydrogen sulfide; hydroxylamine hydrochloride; acetic anhydride; triethylamine; In ethanol; water;

upstream raw materials:

methanol

thymoxyacetonitrile

thymol

Downstream raw materials:

2-(thymoxymethyl)-4-(2'-pyrazinyl)thiazole

2-(thymoxymethyl)-4-(5'-nitro-2'-furyl)thiazole