1-(4-fluoro-phenyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

Base Information

Chemical Name:1-(4-fluoro-phenyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester
CAS No.:1147216-22-5
Molecular Formula:C₁₂H₁₂FN₃O₂
Molecular Weight:249.245
Hs Code.:

Synonyms:1-(4-fluoro-phenyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

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Chemical Property of 1-(4-fluoro-phenyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1-(4-fluoro-phenyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

There total 4 articles about 1-(4-fluoro-phenyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3296-02-4
p-azidofluorobenzene

: 141-97-9
ethyl acetoacetate

: 1147216-22-5
1-(4-fluoro-phenyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

Guidance literature:: With diethylamine; In dimethyl sulfoxide; at 70 ℃; for 18h; Inert atmosphere;

Reference yield:

: 64-17-5
ethanol

: 887035-89-4
1-(4-fluoro-phenyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid

: 1147216-22-5
1-(4-fluoro-phenyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

Guidance literature:: ethanol; 1-(4-fluoro-phenyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid; With sulfuric acid; at 20 - 78 ℃; for 8h;

With sodium hydroxide; In water; pH=10;

Reference yield:

: 1765-93-1
4-fluoroboronic acid

: 141-97-9
ethyl acetoacetate

: 1147216-22-5
1-(4-fluoro-phenyl)-5-methyl-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

Guidance literature:: With piperidine; sodium azide; copper diacetate; In water; dimethyl sulfoxide; at 20 - 80 ℃; for 24h;
DOI:10.1016/j.bmcl.2016.02.059