(8R,9S,13S,14S)-2,4-Dihydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one

Base Information

• Chemical Name: (8R,9S,13S,14S)-2,4-Dihydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one
• CAS No.: 95717-17-2
• Molecular Formula: C₁₈H₂₂O₃
• Molecular Weight: 286.371

Synonyms:(8R,9S,13S,14S)-2,4-Dihydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one

Chemical Property of (8R,9S,13S,14S)-2,4-Dihydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one

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Technology Process of (8R,9S,13S,14S)-2,4-Dihydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one

There total 1 articles about (8R,9S,13S,14S)-2,4-Dihydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

estrone acetate (901-93-9) → Estrone (53-16-7) + Estrone quinol (549-03-1) + (8R,9S,13S,14S)-2,4-Dihydroxy-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one (95717-17-2) + 1,3-dihydroxy-estra-1,3,5(10)-trien-17-one (60966-54-3) + Acetic acid (8R,9S,13S,14S)-4-hydroxy-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-2-yl ester + Acetic acid (8R,9S,13S,14S)-1-hydroxy-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:

With hydrogen fluoride; dihydrogen peroxide; antimony pentafluoride; at -45 ℃; for 0.0125h; Product distribution; various aromatics investigated;

upstream raw materials:

estrone acetate

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