2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptonic acid 3,4,5,7-tetrabenzoate

Base Information

Chemical Name:2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptonic acid 3,4,5,7-tetrabenzoate
CAS No.:120172-79-4
Molecular Formula:C₃₇H₂₈F₃NO₁₁
Molecular Weight:719.625
Hs Code.:

Synonyms:2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptonic acid 3,4,5,7-tetrabenzoate

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Chemical Property of 2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptonic acid 3,4,5,7-tetrabenzoate

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Technology Process of 2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptonic acid 3,4,5,7-tetrabenzoate

There total 4 articles about 2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptonic acid 3,4,5,7-tetrabenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78821-34-8
2,6-dideoxy-2,6-imino-D-glycero-D-ido-heptononitrile

: 120172-79-4
2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptonic acid 3,4,5,7-tetrabenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / triethylamine / ethyl acetate / 18 h / Ambient temperature

2: 89 percent / triethylamine / ethyl acetate / 1.) 0 deg C, 1 h, 2.) room temperature, 21 h

3: 1.) mercuric trifluoroacetate, 2.) N₂O₄ / 1.) 90percent TFA, room temperature, 3.5 h, 2.) room temperature, 1.5 h

With mercury(II) trifluoroacetate; dinitrogen tetraoxide; triethylamine; In ethyl acetate;
DOI:10.1021/jo00272a015

Reference yield:

: 120172-77-2
2,6-dideoxy-2,6-imino-D-glycero-D-ido-heptononitrile 3,4,5,7-tetrabenzoate

: 120172-79-4
2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptonic acid 3,4,5,7-tetrabenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / triethylamine / ethyl acetate / 1.) 0 deg C, 1 h, 2.) room temperature, 21 h

2: 1.) mercuric trifluoroacetate, 2.) N₂O₄ / 1.) 90percent TFA, room temperature, 3.5 h, 2.) room temperature, 1.5 h

With mercury(II) trifluoroacetate; dinitrogen tetraoxide; triethylamine; In ethyl acetate;
DOI:10.1021/jo00272a015

Reference yield:

: 98-88-4
benzoyl chloride

: 120172-79-4
2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptonic acid 3,4,5,7-tetrabenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / triethylamine / ethyl acetate / 18 h / Ambient temperature

2: 89 percent / triethylamine / ethyl acetate / 1.) 0 deg C, 1 h, 2.) room temperature, 21 h

3: 1.) mercuric trifluoroacetate, 2.) N₂O₄ / 1.) 90percent TFA, room temperature, 3.5 h, 2.) room temperature, 1.5 h

With mercury(II) trifluoroacetate; dinitrogen tetraoxide; triethylamine; In ethyl acetate;
DOI:10.1021/jo00272a015