5-tert-butyl-2-oxocyclohexanecarboxylic acid

Base Information

Chemical Name:5-tert-butyl-2-oxocyclohexanecarboxylic acid
CAS No.:42031-70-9
Molecular Formula:C₁₁H₁₈O₃
Molecular Weight:198.262
Hs Code.:

Synonyms:5-tert-butyl-2-oxocyclohexanecarboxylic acid

Suppliers and Price of 5-tert-butyl-2-oxocyclohexanecarboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 5-tert-butyl-2-oxocyclohexanecarboxylic acid

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

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Technology Process of 5-tert-butyl-2-oxocyclohexanecarboxylic acid

There total 4 articles about 5-tert-butyl-2-oxocyclohexanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4861-79-4
magnesium methyl carbonate

: 98-53-3
4-tercbutyl-cyclohexanone

: 42031-70-9
5-tert-butyl-2-oxocyclohexanecarboxylic acid

: C₁₂H₁₈O₅

Guidance literature:: In N,N-dimethyl-formamide; at 130 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tet.2015.02.060

Reference yield:

: 4861-79-4
magnesium methyl carbonate

: 98-53-3
4-tercbutyl-cyclohexanone

: 42031-70-9
5-tert-butyl-2-oxocyclohexanecarboxylic acid

: C₁₂H₁₈O₅

Guidance literature:: In N,N-dimethyl-formamide; at 130 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol5024129

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 98-53-3
4-tercbutyl-cyclohexanone

: 42031-70-9
5-tert-butyl-2-oxocyclohexanecarboxylic acid

Guidance literature:: With n-butyllithium; 1,10-Phenanthroline; diisopropylamine; Yield given. Multistep reaction; 1.) ether, 1 deg C, 1 h, 2.) 1 deg C, 35 min, 1 deg C to room temp. 30 min;
DOI:10.1021/jo00172a011