2-(3,5-dimethyl-1H-pyrazol-1-yl)-4-{4-nitrophenyl}-1,3-thiazole

Base Information

• Chemical Name: 2-(3,5-dimethyl-1H-pyrazol-1-yl)-4-{4-nitrophenyl}-1,3-thiazole
• CAS No.: 106691-15-0
• Molecular Formula: C₁₄H₁₂N₄O₂S
• Molecular Weight: 300.341
• Mol file: 106691-15-0.mol

Synonyms:2-(3,5-dimethyl-1H-pyrazol-1-yl)-4-(4-nitrophenyl)thiazole

Chemical Property of 2-(3,5-dimethyl-1H-pyrazol-1-yl)-4-{4-nitrophenyl}-1,3-thiazole

Chemical Property:

Purity/Quality:

2-(3,5-DIMETHYL-1H-PYRAZOL-1-YL)-4-(4-NITROPHENYL)-1,3-THIAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

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Technology Process of 2-(3,5-dimethyl-1H-pyrazol-1-yl)-4-{4-nitrophenyl}-1,3-thiazole

There total 5 articles about 2-(3,5-dimethyl-1H-pyrazol-1-yl)-4-{4-nitrophenyl}-1,3-thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

3,5-dimethyl-1H-pyrazole-1-carbothioamide (1124-15-8) + 4-Nitrophenacyl bromide (99-81-0) → 2-(3,5-dimethyl-1H-pyrazol-1-yl)-4-(4-nitrophenyl)thiazole (106691-15-0)

Guidance literature:

With sodium carbonate; In neat (no solvent, solid phase); at 20 ℃; for 0.0833333h; Green chemistry;

DOI:10.1080/17415993.2012.711331

Reference yield: 93.0%

3,5-dimethyl-1H-pyrazole-1-carbothioamide (1124-15-8) + 2-iodo-1-(4-nitrophenyl)ethanone (110944-98-4) → 2-(3,5-dimethyl-1H-pyrazol-1-yl)-4-(4-nitrophenyl)thiazole (106691-15-0)

Guidance literature:

With sodium carbonate; In neat (no solvent, solid phase); at 20 ℃; for 0.0833333h; Green chemistry;

DOI:10.1080/17415993.2012.711331

Reference yield:

3,5-dimethyl-1H-pyrazole-1-carbothioamide (1124-15-8) + 2,2-dibromo-1-(4-nitro-phenyl)-ethanone (21566-36-9) → 2-(3,5-dimethyl-1H-pyrazol-1-yl)-4-(4-nitrophenyl)thiazole (106691-15-0)

Guidance literature:

In ethanol; at 20 ℃; for 0.25h;

DOI:10.1080/00397910701462476

upstream raw materials:

3,5-dimethyl-1H-pyrazole-1-carbothioamide

4-Nitrophenacyl bromide

2-Hydrazino-4-(4-nitrophenyl)thiazole

acetylacetone

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