((5S,6R,10S)-10-(4-methoxyphenyl)-4-oxo-3-phenyl-2-thioxo-1-thia-3-azaspiro[4.5]dec-7-en-6-yl)acetaldehyde

Base Information

• Chemical Name: ((5S,6R,10S)-10-(4-methoxyphenyl)-4-oxo-3-phenyl-2-thioxo-1-thia-3-azaspiro[4.5]dec-7-en-6-yl)acetaldehyde
• CAS No.: 1426097-56-4
• Molecular Formula: C₂₃H₂₁NO₃S₂
• Molecular Weight: 423.557

Synonyms:((5S,6R,10S)-10-(4-methoxyphenyl)-4-oxo-3-phenyl-2-thioxo-1-thia-3-azaspiro[4.5]dec-7-en-6-yl)acetaldehyde

Chemical Property of ((5S,6R,10S)-10-(4-methoxyphenyl)-4-oxo-3-phenyl-2-thioxo-1-thia-3-azaspiro[4.5]dec-7-en-6-yl)acetaldehyde

Chemical Property:

Purity/Quality:

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Technology Process of ((5S,6R,10S)-10-(4-methoxyphenyl)-4-oxo-3-phenyl-2-thioxo-1-thia-3-azaspiro[4.5]dec-7-en-6-yl)acetaldehyde

There total 1 articles about ((5S,6R,10S)-10-(4-methoxyphenyl)-4-oxo-3-phenyl-2-thioxo-1-thia-3-azaspiro[4.5]dec-7-en-6-yl)acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

2,4-hexadienal (80466-34-8,4488-48-6) + (5E,5Z)-5-(4-methoxybenzylidene)-3-phenyl-2-thioxo-1,3-thiazolidin-4-one (55111-70-1) → ((5S,6R,10S)-10-(4-methoxyphenyl)-4-oxo-3-phenyl-2-thioxo-1-thia-3-azaspiro[4.5]dec-7-en-6-yl)acetaldehyde (1426097-56-4)

Guidance literature:

With (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; o-fluoro-benzoic acid; In chloroform-d1; at 50 ℃; for 72h; stereoselective reaction;

DOI:10.1039/c3cc00023k

Reference yield:

((5S,6R,10S)-10-(4-methoxyphenyl)-4-oxo-3-phenyl-2-thioxo-1-thia-3-azaspiro[4.5]dec-7-en-6-yl)acetaldehyde (1426097-56-4) + methyl (triphenylphosphoranylidene)acetate (21204-67-1,2605-67-6) → C26H25NO4S2

Guidance literature:

In tetrahydrofuran; at 20 ℃;

DOI:10.1039/c3cc00023k

upstream raw materials:

2,4-hexadienal

(5E,5Z)-5-(4-methoxybenzylidene)-3-phenyl-2-thioxo-1,3-thiazolidin-4-one

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