6α-methylprednisolone-17α,21-methyl orthobenzoate

Base Information

Chemical Name:6α-methylprednisolone-17α,21-methyl orthobenzoate
CAS No.:85198-29-4
Molecular Formula:C₃₀H₃₆O₆
Molecular Weight:492.612
Hs Code.:

Synonyms:6α-methylprednisolone-17α,21-methyl orthobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6α-methylprednisolone-17α,21-methyl orthobenzoate

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Technology Process of 6α-methylprednisolone-17α,21-methyl orthobenzoate

There total 2 articles about 6α-methylprednisolone-17α,21-methyl orthobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 103744-18-9
(6S,8S,9S,10R,11S,13S,14S,17S)-11-Hydroxy-17-(2-hydroxy-acetyl)-6,10,13-trimethyl-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-cyclopenta[a]phenanthren-3-one

: 707-07-3
orthobenzoic acid trimethyl ester

: 85198-29-4
6α-methylprednisolone-17α,21-methyl orthobenzoate

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 85 ℃; for 1.5h;
DOI:10.1055/s-1982-30048

Reference yield:

: 83-43-2
Methylprednisolone

: 707-07-3
orthobenzoic acid trimethyl ester

: 85198-29-4
6α-methylprednisolone-17α,21-methyl orthobenzoate

Guidance literature:: With sodium carbonate; toluene-4-sulfonic acid; Yield given. Multistep reaction; 1.) DMF, 70-90 deg C, 2.) DMF, water, ethyl acetate;
DOI:10.1248/cpb.31.12