1-phenyl-5,6-dihydrobenzoindolizine

Base Information

• Chemical Name: 1-phenyl-5,6-dihydrobenzoindolizine
• CAS No.: 145474-59-5
• Molecular Formula: C₁₈H₁₅N
• Molecular Weight: 245.324

Synonyms:1-phenyl-5,6-dihydrobenzoindolizine

Chemical Property of 1-phenyl-5,6-dihydrobenzoindolizine

Chemical Property:

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Technology Process of 1-phenyl-5,6-dihydrobenzoindolizine

There total 9 articles about 1-phenyl-5,6-dihydrobenzoindolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1,2,3,4-tetrahydroisoquinoline (91-21-4) + (Z)-2-methyl-5-phenylpent-2-en-4-ynal (127743-21-9) → 1-phenyl-5,6-dihydrobenzoindolizine (145474-59-5)

Guidance literature:

With trifluoroacetic acid; In toluene; at 130 ℃; for 5h; Temperature; Schlenk technique;

Reference yield: 57.0%

2-cinnamyl-1,2,3,4-tetrahydroisoquinoline (145474-49-3) → 1-phenyl-5,6-dihydrobenzoindolizine (145474-59-5)

Guidance literature:

With silver carbonate; In xylene; at 140 ℃; for 18h;

DOI:10.1016/S0040-4020(01)81190-X

Reference yield:

1-(1-phenylpropa-1,2-dienyl)-1,2,3,4-tetrahydroisoquinoline (1423919-30-5) → 1-phenyl-5,6-dihydrobenzoindolizine (145474-59-5)

Guidance literature:

With silver(I) acetate; In dichloromethane; at 20 ℃; for 14h; Darkness;

DOI:10.1039/c2ra22823h

upstream raw materials:

2-cinnamyl-1,2,3,4-tetrahydroisoquinoline

2-bromophenyl 1-[2'-(2''-bromophenyl)ethyl]-4-phenylpyrrole-2-carboxylate

1,2,3,4-tetrahydroisoquinoline

Cinnamyl bromide

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