1-<2-azido-2-deoxy-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl>-5-benzylideneamino-4-cyanoimidazole

Base Information

Chemical Name:1-<2-azido-2-deoxy-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl>-5-benzylideneamino-4-cyanoimidazole
CAS No.:125338-99-0
Molecular Formula:C₂₈H₄₁N₇O₄Si₂
Molecular Weight:595.849
Hs Code.:

Synonyms:1-<2-azido-2-deoxy-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl>-5-benzylideneamino-4-cyanoimidazole

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Chemical Property of 1-<2-azido-2-deoxy-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl>-5-benzylideneamino-4-cyanoimidazole

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Technology Process of 1-<2-azido-2-deoxy-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl>-5-benzylideneamino-4-cyanoimidazole

There total 6 articles about 1-<2-azido-2-deoxy-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl>-5-benzylideneamino-4-cyanoimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 125338-94-5
5-benzylideneamino-4-cyano-1-<2-O-triflyl-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>imidazole

: 125338-99-0
1-<2-azido-2-deoxy-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl>-5-benzylideneamino-4-cyanoimidazole

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; for 24h; Ambient temperature;
DOI:10.1248/cpb.37.1604

Reference yield:

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 125338-99-0
1-<2-azido-2-deoxy-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl>-5-benzylideneamino-4-cyanoimidazole

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / dimethylformamide; various solvent(s) / 0.67 h / Ambient temperature

2: 94 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

3: 75 percent / 4-dimethylaminopyridine, pyridine / triethylamine / 0.5 h / Ambient temperature

4: 83 percent / NaN₃ / dimethylformamide / 24 h / Ambient temperature

With pyridine; dmap; sodium azide; toluene-4-sulfonic acid; In triethylamine; N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.37.1604

Reference yield:

: 100-52-7
benzaldehyde

: 125338-99-0
1-<2-azido-2-deoxy-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl>-5-benzylideneamino-4-cyanoimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

2: 75 percent / 4-dimethylaminopyridine, pyridine / triethylamine / 0.5 h / Ambient temperature

3: 83 percent / NaN₃ / dimethylformamide / 24 h / Ambient temperature

With pyridine; dmap; sodium azide; toluene-4-sulfonic acid; In triethylamine; N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.37.1604