4-Aminomethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Base Information

Chemical Name:4-Aminomethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion
CAS No.:286374-82-1
Molecular Formula:C₁₁H₉F₃N₂S₂
Molecular Weight:290.333
Hs Code.:

Synonyms:4-Aminomethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

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Chemical Property of 4-Aminomethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

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Technology Process of 4-Aminomethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

There total 5 articles about 4-Aminomethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 286374-81-0
2-[2-Thioxo-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-4-ylmethyl]isoindolin-1,3-dion

: 286374-82-1
4-Aminomethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Guidance literature:: With hydrazine hydrate; In ethanol; for 1h; Heating;

Reference yield:

: 98-16-8
3-trifluoromethylaniline

: 286374-82-1
4-Aminomethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Guidance literature:: Multi-step reaction with 5 steps

1: 30.12 g / 20 °C

2: 80 percent / methanol; acetone / 2 h / 20 °C

3: 22.08 g / HCl / ethyl acetate / 2 h / Heating

4: 92 percent / 18-crown-6 / toluene / 2 h / Heating

5: 93 percent / N₂H₄*H₂O / ethanol / 1 h / Heating

With hydrogenchloride; hydrazine hydrate; 18-crown-6 ether; In methanol; ethanol; ethyl acetate; acetone; toluene; 1: Addition / 2: Cyclization / 3: Dehydration / 4: Substitution / 5: hydrazinolysis;

Reference yield:

: 286374-52-5
4-Chlormethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

: 286374-82-1
4-Aminomethyl-3-(3-trifluormethylphenyl)-2,3-dihydro-1,3-thiazol-2-thion

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 18-crown-6 / toluene / 2 h / Heating

2: 93 percent / N₂H₄*H₂O / ethanol / 1 h / Heating

With hydrazine hydrate; 18-crown-6 ether; In ethanol; toluene; 1: Substitution / 2: hydrazinolysis;