(C₁₂H₈N₂)Pd(CH₂CH₂C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)= [(C₁₂H₈N₂)Pd(CH₂CH₂C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4

Base Information

• Chemical Name: (C₁₂H₈N₂)Pd(CH₂CH₂C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)= [(C₁₂H₈N₂)Pd(CH₂CH₂C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4
• CAS No.: 175858-05-6
• Molecular Formula: C₁₇H₁₅N₂O₂Pd*C₃₂H₁₂BF₂₄
• Molecular Weight: 1248.96

Synonyms:(C₁₂H₈N₂)Pd(CH₂CH₂C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)= [(C₁₂H₈N₂)Pd(CH₂CH₂C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4

Chemical Property of (C₁₂H₈N₂)Pd(CH₂CH₂C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)= [(C₁₂H₈N₂)Pd(CH₂CH₂C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4

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Technology Process of (C₁₂H₈N₂)Pd(CH₂CH₂C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)= [(C₁₂H₈N₂)Pd(CH₂CH₂C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4

There total 1 articles about (C₁₂H₈N₂)Pd(CH₂CH₂C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)= [(C₁₂H₈N₂)Pd(CH₂CH₂C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.7%

ethene (74-85-1) + [Pd(CH3)(CO)(1,10-phenanthroline)][B(3,5-(CF3)2-C6H3)4] (160498-14-6) + (C12H8N2)Pd(CH2CH2C(CH3)O)(1+)*B(C6H3(CF3)2)4(1-) = [(C12H8N2)Pd(CH2CH2C(CH3)O)]B(C6H3(CF3)2)4 → (C12H8N2)Pd(CH3)(C2H4)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(CH3)(C2H4)]B(C6H3(CF3)2)4 (160498-12-4) + (C12H8N2)Pd(CH2CH2C(O)CH3)(CO)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(CH2CH2C(O)CH3)(CO)]B(C6H3(CF3)2)4 (175858-05-6) + (C12H8N2)Pd(C(O)CH2CH2C(CH3)O)(1+)*B(C6H3(CF3)2)4(1-) = [(C12H8N2)Pd(C(O)CH2CH2C(CH3)O)]B(C6H3(CF3)2)4 + (C12H8N2)Pd(CH2CH2C(O)CH3)(C2H4)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(CH2CH2C(O)CH3)(C2H4)]B(C6H3(CF3)2)4 (160498-05-5) + (C12H8N2)Pd(C(O)CH2CH2C(O)CH3)(C2H4)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(C(O)CH2CH2C(O)CH3)(C2H4)]B(C6H3(CF3)2)4 (160498-06-6)

Guidance literature:

In dichloromethane-d2; (Ar); -83°C; detected by NMR;

DOI:10.1021/ja953276t

Reference yield: 70.0%

(C12H8N2)Pd(CH2CH2C(O)CH3)(CO)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(CH2CH2C(O)CH3)(CO)]B(C6H3(CF3)2)4 (175858-05-6) + carbon monoxide (201230-82-2) → (C12H8N2)Pd(C(O)CH2CH2C(CH3)O)(1+)*B(C6H3(CF3)2)4(1-) = [(C12H8N2)Pd(C(O)CH2CH2C(CH3)O)]B(C6H3(CF3)2)4 + (C12H8N2)Pd(C(O)CH2CH2C(O)CH3)(CO)(1+)*B(C6H3(CF3)2)4(1-)= [(C12H8N2)Pd(C(O)CH2CH2C(O)CH3)(CO)]B(C6H3(CF3)2)4 (175858-07-8)

Guidance literature:

In dichloromethane-d2; (Ar); -78°C; Kinetics;

DOI:10.1021/ja953276t

upstream raw materials:

ethene

[Pd(CH₃)(CO)(1,10-phenanthroline)][B(3,5-(CF₃)2-C₆H₃)4]

Downstream raw materials:

(C₁₂H₈N₂)Pd(C(O)CH₂CH₂C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)= [(C₁₂H₈N₂)Pd(C(O)CH₂CH₂C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4

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