[3-({[tert-butyl(diphenyl)silyl]oxy}methyl)-5-isopropoxyphenyl]methanol

Base Information

• Chemical Name: [3-({[tert-butyl(diphenyl)silyl]oxy}methyl)-5-isopropoxyphenyl]methanol
• CAS No.: 888741-15-9
• Molecular Formula: C₂₇H₃₄O₃Si
• Molecular Weight: 434.651

Synonyms:[3-({[tert-butyl(diphenyl)silyl]oxy}methyl)-5-isopropoxyphenyl]methanol

Chemical Property of [3-({[tert-butyl(diphenyl)silyl]oxy}methyl)-5-isopropoxyphenyl]methanol

Chemical Property:

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Technology Process of [3-({[tert-butyl(diphenyl)silyl]oxy}methyl)-5-isopropoxyphenyl]methanol

There total 1 articles about [3-({[tert-butyl(diphenyl)silyl]oxy}methyl)-5-isopropoxyphenyl]methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

(5-isopropoxy-1,3-phenylene)dimethanol + sodium hydrogencarbonate (144-55-8) + tert-butylchlorodiphenylsilane (58479-61-1) → [3-({[tert-butyl(diphenyl)silyl]oxy}methyl)-5-isopropoxyphenyl]methanol (888741-15-9)

Guidance literature:

With dmap; triethylamine; In dichloromethane;

Reference yield: 90.0%

[3-({[tert-butyl(diphenyl)silyl]oxy}methyl)-5-isopropoxyphenyl]methanol (888741-15-9) + 1,1'-(Azodicarbonyl)dipiperidin (10465-81-3,871024-86-1) + sodium hydrogencarbonate (144-55-8) + 2,4-dichlorophenol (120-83-2,40477-79-0) → {3-[(2,4-dichlorophenoxy)methyl]-5-isopropoxyphenyl}methanol (888741-16-0)

Guidance literature:

With tributylphosphine; tetrabutyl ammonium fluoride; In tetrahydrofuran; di-isopropyl ether;

Reference yield: 72.0%

(2-(tetrahydro-furan-2-yl)-ethanol) (33606-34-7) + [3-({[tert-butyl(diphenyl)silyl]oxy}methyl)-5-isopropoxyphenyl]methanol (888741-15-9) + triethyl phosphonoacetic acid → ethyl 3-[3-({[tert-butyl(diphenyl)silyl]oxy}methyl)-5-isopropoxyphenyl]propanoate (888741-17-1)

Guidance literature:

With manganese dioxide; palladium-carbon; In tetrahydrofuran; tetrahydrofuran-toluene; water; N,N-dimethyl-formamide;

upstream raw materials:

sodium hydrogencarbonate

tert-butylchlorodiphenylsilane

Downstream raw materials:

{3-[(2,4-dichlorophenoxy)methyl]-5-isopropoxyphenyl}methanol

ethyl 3-[3-({[tert-butyl(diphenyl)silyl]oxy}methyl)-5-isopropoxyphenyl]propanoate

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