exo-2-<3,4-bis(benzyloxy)phenyl>-2-hydroxy-3-(hydroxyimino)bicyclo<2.2.1>heptane

Base Information

Chemical Name:exo-2-<3,4-bis(benzyloxy)phenyl>-2-hydroxy-3-(hydroxyimino)bicyclo<2.2.1>heptane
CAS No.:118891-89-7
Molecular Formula:C₂₇H₂₇NO₄
Molecular Weight:429.516
Hs Code.:

Synonyms:exo-2-<3,4-bis(benzyloxy)phenyl>-2-hydroxy-3-(hydroxyimino)bicyclo<2.2.1>heptane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of exo-2-<3,4-bis(benzyloxy)phenyl>-2-hydroxy-3-(hydroxyimino)bicyclo<2.2.1>heptane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of exo-2-<3,4-bis(benzyloxy)phenyl>-2-hydroxy-3-(hydroxyimino)bicyclo<2.2.1>heptane

There total 1 articles about exo-2-<3,4-bis(benzyloxy)phenyl>-2-hydroxy-3-(hydroxyimino)bicyclo<2.2.1>heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28043-14-3
3-(hydroxyimino)-2-oxobicyclo<2.2.1>heptane

: 16047-57-7
<3,4-bis(benzyloxy)phenyl>magnesium bromide

: 118891-89-7
exo-2-<3,4-bis(benzyloxy)phenyl>-2-hydroxy-3-(hydroxyimino)bicyclo<2.2.1>heptane

Guidance literature:: In diethyl ether; for 7h; Yield given; Heating;
DOI:10.1021/jm00124a020

Reference yield:

: 118891-89-7
exo-2-<3,4-bis(benzyloxy)phenyl>-2-hydroxy-3-(hydroxyimino)bicyclo<2.2.1>heptane

: 118891-94-4
endo-3-amino-exo-2-(3,4-dihydroxyphenyl)-2-hydroxy-bicyclo<2.2.1>heptane

Guidance literature:: Multi-step reaction with 2 steps

1: LAH / diethyl ether / 6 h / Heating

2: H₂ / 10percent Pd-C / CH₂Cl₂; ethanol / 50 °C / 760 Torr

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jm00124a020

Reference yield:

: 118891-89-7
exo-2-<3,4-bis(benzyloxy)phenyl>-2-hydroxy-3-(hydroxyimino)bicyclo<2.2.1>heptane

: 118891-95-5
exo-2-(3,4-dihydroxyphenyl)-2-hydroxy-endo-3-(isopropylamino)bicyclo<2.2.1>heptane

Guidance literature:: Multi-step reaction with 2 steps

1: LAH / diethyl ether / 6 h / Heating

2: 2.) H₂ / 2.) 10percent Pd-C / 1.) MeOH, 14 h, 2.) 50 deg C, 760 torr, 7 h

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether;
DOI:10.1021/jm00124a020