C₃₄H₄₀NO₄⁽¹⁺⁾*I^(1-)

Base Information

• Chemical Name: C₃₄H₄₀NO₄⁽¹⁺⁾*I^(1-)
• CAS No.: 1353554-61-6
• Molecular Formula: C₃₄H₄₀NO₄*I
• Molecular Weight: 653.6
• Mol file: 1353554-61-6.mol

Synonyms:C₃₄H₄₀NO₄⁽¹⁺⁾*I^(1-)

Chemical Property of C₃₄H₄₀NO₄⁽¹⁺⁾*I^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₄₀NO₄⁽¹⁺⁾*I^(1-)

There total 8 articles about C₃₄H₄₀NO₄⁽¹⁺⁾*I^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

C31H33NO4 (1353554-59-2) + 1-iodo-propane (107-08-4) → C34H40NO4(1+)*I(1-) (1353554-61-6)

Guidance literature:

at 80 ℃; for 6h; Inert atmosphere;

Reference yield:

3,4-dimethoxyaniline (6315-89-5) → C34H40NO4(1+)*I(1-) (1353554-61-6)

Guidance literature:

Multi-step reaction with 6 steps

1.1: hydrogenchloride / ethanol; water / 12 h / Inert atmosphere; Reflux

1.2: pH 9

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 5 h / 100 °C / Inert atmosphere

3.1: hydrogen; acetic acid / palladium 10% on activated carbon / 20 - 60 °C / 760.05 Torr

4.1: triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere

5.1: potassium carbonate / palladium diacetate; XPhos / 1,4-dioxane; water / 3 h / 95 °C / Inert atmosphere

6.1: 6 h / 80 °C / Inert atmosphere

With hydrogenchloride; hydrogen; potassium carbonate; acetic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; palladium diacetate; XPhos; In 1,4-dioxane; ethanol; dichloromethane; water; 2.1: Suzuki Coupling / 5.1: Suzuki Coupling;

Reference yield:

3-bromo-6,7-dimethoxyquinoline (850352-73-7) → C34H40NO4(1+)*I(1-) (1353554-61-6)

Guidance literature:

Multi-step reaction with 5 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 5 h / 100 °C / Inert atmosphere

2: hydrogen; acetic acid / palladium 10% on activated carbon / 20 - 60 °C / 760.05 Torr

3: triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere

4: potassium carbonate / palladium diacetate; XPhos / 1,4-dioxane; water / 3 h / 95 °C / Inert atmosphere

5: 6 h / 80 °C / Inert atmosphere

With hydrogen; potassium carbonate; acetic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; palladium diacetate; XPhos; In 1,4-dioxane; dichloromethane; water; 1: Suzuki Coupling / 4: Suzuki Coupling;

upstream raw materials:

3,4-dimethoxyaniline

C₃₁H₃₃NO₄

1-iodo-propane

3-bromo-6,7-dimethoxyquinoline

Refernces