N-benzyloxycarbonyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamid

Base Information

Chemical Name:N-benzyloxycarbonyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamid
CAS No.:75509-34-1
Molecular Formula:C₃₆H₄₃N₇O₈S₂
Molecular Weight:765.912
Hs Code.:

Synonyms:N-benzyloxycarbonyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyloxycarbonyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamid

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Technology Process of N-benzyloxycarbonyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamid

There total 4 articles about N-benzyloxycarbonyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 75509-33-0
S-benyl-L-cysteinylglycylglycinamide

: 75509-29-4
N-benzyloxycarbonyl-S-benzyl-L-cysteinylglycylglycine succinimido-ester

: 75509-34-1
N-benzyloxycarbonyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamid

Guidance literature:: In 1,4-dioxane; for 24h; Ambient temperature;
DOI:10.1039/DT9800001228

Reference yield:

: 3401-57-8
N-benzyloxycarbonyl-S-benzyl-L-cysteine succinimido-ester

: 75509-34-1
N-benzyloxycarbonyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamid

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / dioxane / 24 h / Ambient temperature

2: 91 percent / 45percent HBr / acetic acid / 0.83 h / 20 °C

3: 70 percent / dioxane / 24 h / Ambient temperature

With hydrogen bromide; In 1,4-dioxane; acetic acid;
DOI:10.1039/DT9800001228

Reference yield:

: 75509-30-7
N-benzyloxycarbonyl-S-benzyl-L-cysteinylglycylglycine

: 75509-34-1
N-benzyloxycarbonyl-S-benzyl-L-cysteinyldiglycyl-S-benzyl-L-cysteinylglycylglycinamid

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / N,N'-dicyclohexylcarbodi-imide / dimethylformamide / 24 h / 0 - 25 °C

2: 70 percent / dioxane / 24 h / Ambient temperature

With dicyclohexyl-carbodiimide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/DT9800001228