Ru(III)[4'-(4-dimethylaminophenyl)-2,2': 6',2''-terpyridine]Cl₃

Base Information

Chemical Name:Ru(III)[4'-(4-dimethylaminophenyl)-2,2': 6',2''-terpyridine]Cl₃
CAS No.:405149-91-9
Molecular Formula:C₂₃H₂₀Cl₃N₄Ru
Molecular Weight:559.868
Hs Code.:

Ru(III)[4'-(4-dimethylaminophenyl)-2,2': 6',2''-terpyridine]Cl<sub>3</sub>

Synonyms:Ru(III)[4'-(4-dimethylaminophenyl)-2,2': 6',2''-terpyridine]Cl₃

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Chemical Property of Ru(III)[4'-(4-dimethylaminophenyl)-2,2': 6',2''-terpyridine]Cl₃

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Technology Process of Ru(III)[4'-(4-dimethylaminophenyl)-2,2': 6',2''-terpyridine]Cl₃

There total 4 articles about Ru(III)[4'-(4-dimethylaminophenyl)-2,2': 6',2''-terpyridine]Cl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.2%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 362595-93-5
4’-(4-N,N-dimethylaminophenyl)-2,2’:6’,2’’-terpyridine

: 405149-91-9
Ru(III)[4'-(4-dimethylaminophenyl)-2,2': 6',2''-terpyridine]Cl₃

Guidance literature:: In ethanol; dichloromethane; mixt. of RuCl3*3H2O and ligand in CH2Cl2 and EtOH was refluxed for 1 h, cooled to room temp.; filtered off, washed with H2O, EtOH, CH2Cl2, Et2O, dried in air;
DOI:10.1021/ja011069p

Reference yield:

: 63767-78-2
ruthenium trichloride

: 362595-93-5
4’-(4-N,N-dimethylaminophenyl)-2,2’:6’,2’’-terpyridine

: 405149-91-9
Ru(III)[4'-(4-dimethylaminophenyl)-2,2': 6',2''-terpyridine]Cl₃

Guidance literature:: In methanol; for 3h; Inert atmosphere; Reflux;
DOI:10.1080/00958972.2021.1924368

Reference yield:

: 1122-62-9
2-acetylpyridine

: 100-10-7
4-dimethylamino-benzaldehyde

: 405149-91-9
Ru(III)[4'-(4-dimethylaminophenyl)-2,2': 6',2''-terpyridine]Cl₃

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide; ammonia / ethanol / 16 h / 20 °C / Inert atmosphere

2: methanol / 3 h / Inert atmosphere; Reflux

With ammonia; potassium hydroxide; In methanol; ethanol;
DOI:10.1080/00958972.2021.1924368