N-(2-(2-(4-chlorobenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide

Base Information

Chemical Name:N-(2-(2-(4-chlorobenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide
CAS No.:901142-19-6
Molecular Formula:C₂₃H₁₈ClN₃O₂S₂
Molecular Weight:468
Hs Code.:

Synonyms:N-(2-(2-(4-chlorobenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide

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Chemical Property of N-(2-(2-(4-chlorobenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide

Chemical Property:

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Technology Process of N-(2-(2-(4-chlorobenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide

There total 3 articles about N-(2-(2-(4-chlorobenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 901116-33-4
C₁₆H₁₄ClN₃OS₂

: 98-88-4
benzoyl chloride

: 901142-19-6
N-(2-(2-(4-chlorobenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1016/j.bmcl.2010.12.124

Reference yield:

: 99585-88-3
2-chloro-N-(4-chlorobenzyl)acetamide

: 901142-19-6
N-(2-(2-(4-chlorobenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 4 h / Reflux

2: sodium hydrogencarbonate / dichloromethane / 6 h / 20 °C

With sodium hydrogencarbonate; potassium carbonate; In dichloromethane; acetone;
DOI:10.1016/j.bmcl.2010.12.124

Reference yield:

: 104-86-9
4-chlorobenzylamine

: 901142-19-6
N-(2-(2-(4-chlorobenzylamino)-2-oxoethylthio)benzothiazol-6-yl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dichloromethane / 0 °C / Reflux

2: potassium carbonate / acetone / 4 h / Reflux

3: sodium hydrogencarbonate / dichloromethane / 6 h / 20 °C

With sodium hydrogencarbonate; potassium carbonate; In dichloromethane; acetone;
DOI:10.1016/j.bmcl.2010.12.124