N-(5-benzylthio-2-chlorophenyl)-N'-(3-methylthiophenyl)-N'-methyl-guanidine hydrochloride

Base Information

Chemical Name:N-(5-benzylthio-2-chlorophenyl)-N'-(3-methylthiophenyl)-N'-methyl-guanidine hydrochloride
CAS No.:917894-08-7
Molecular Formula:C₂₂H₂₂ClN₃S₂*ClH
Molecular Weight:464.483
Hs Code.:

Synonyms:N-(5-benzylthio-2-chlorophenyl)-N'-(3-methylthiophenyl)-N'-methyl-guanidine hydrochloride

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Chemical Property of N-(5-benzylthio-2-chlorophenyl)-N'-(3-methylthiophenyl)-N'-methyl-guanidine hydrochloride

Chemical Property:

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Technology Process of N-(5-benzylthio-2-chlorophenyl)-N'-(3-methylthiophenyl)-N'-methyl-guanidine hydrochloride

There total 5 articles about N-(5-benzylthio-2-chlorophenyl)-N'-(3-methylthiophenyl)-N'-methyl-guanidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 917894-07-6
2-chloro-5-S-benzyl-thioaniline hydrochloride

: 222734-73-8
N-methyl-N-(3-(methylthio)phenyl)cyanamide

: 917894-08-7
N-(5-benzylthio-2-chlorophenyl)-N'-(3-methylthiophenyl)-N'-methyl-guanidine hydrochloride

Guidance literature:: at 160 ℃; for 3h; sealed flask;

Reference yield:

: 97-08-5
3-nitro-4-chlorosulfonyl chloride

: 917894-08-7
N-(5-benzylthio-2-chlorophenyl)-N'-(3-methylthiophenyl)-N'-methyl-guanidine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; tin(ll) chloride / water / 1.25 h / 0 °C / Heating / reflux

1.2: 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0 °C

2.2: 1 h / 0 - 20 °C

3.1: hydrogenchloride / diethyl ether / 0 °C

3.2: 1 h / 0 - 20 °C

4.1: 3 h / 160 °C / sealed flask

With hydrogenchloride; n-butyllithium; tin(ll) chloride; In tetrahydrofuran; diethyl ether; hexane; water;

Reference yield:

: 917894-06-5
2-chloro-5-S-benzyl-thioaniline

: 917894-08-7
N-(5-benzylthio-2-chlorophenyl)-N'-(3-methylthiophenyl)-N'-methyl-guanidine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / diethyl ether / 0 °C

1.2: 1 h / 0 - 20 °C

2.1: 3 h / 160 °C / sealed flask

With hydrogenchloride; In diethyl ether;