N-(2-chloro-5-(S-2-fluoroethyl)thiophenyl)-N'-(3-methylthiophenyl)-N'-methyl guanidine

Base Information

Chemical Name:N-(2-chloro-5-(S-2-fluoroethyl)thiophenyl)-N'-(3-methylthiophenyl)-N'-methyl guanidine
CAS No.:917894-11-2
Molecular Formula:C₁₇H₁₉ClFN₃S₂
Molecular Weight:383.941
Hs Code.:

Synonyms:N-(2-chloro-5-(S-2-fluoroethyl)thiophenyl)-N'-(3-methylthiophenyl)-N'-methyl guanidine

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Chemical Property of N-(2-chloro-5-(S-2-fluoroethyl)thiophenyl)-N'-(3-methylthiophenyl)-N'-methyl guanidine

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Technology Process of N-(2-chloro-5-(S-2-fluoroethyl)thiophenyl)-N'-(3-methylthiophenyl)-N'-methyl guanidine

There total 16 articles about N-(2-chloro-5-(S-2-fluoroethyl)thiophenyl)-N'-(3-methylthiophenyl)-N'-methyl guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.7%

: 1349064-27-2
1,1’-(disulfanediylbis(6-chloro-1,3-phenylene))bis(3-methyl-3-(3-(methylthio)phenyl)guanidine)

: 383-50-6
2-fluoroethyl tosylate

: 917894-11-2
N-(2-chloro-5-(S-2-fluoroethyl)thiophenyl)-N'-(3-methylthiophenyl)-N'-methyl guanidine

Guidance literature:: With solid phase supported borohydride; In ethanol; at 60 ℃; for 17h; Product distribution / selectivity; Inert atmosphere;

Reference yield: 68.0%

: 917894-09-8
N-(2-chloro-5-mercaptophenyl)-N'-(3-methylthiophenyl)-N'-methyl-guanidine hydrochloride

: 383-50-6
2-fluoroethyl tosylate

: 917894-11-2
N-(2-chloro-5-(S-2-fluoroethyl)thiophenyl)-N'-(3-methylthiophenyl)-N'-methyl guanidine

Guidance literature:: N-(2-chloro-5-mercaptophenyl)-N'-(3-methylthiophenyl)-N'-methyl-guanidine hydrochloride; With potassium carbonate; In acetone;

2-fluoroethyl tosylate; In acetone; for 72h; Heating / reflux;