(1r,4r)-4-((4-(2H-indazol-4-yl)-6-morpholino-1,3,5-triazine-2-yl)oxy)-N,N-dimethycyclohexanecarboxamide hydrochloride

Base Information

Chemical Name:(1r,4r)-4-((4-(2H-indazol-4-yl)-6-morpholino-1,3,5-triazine-2-yl)oxy)-N,N-dimethycyclohexanecarboxamide hydrochloride
CAS No.:1542268-06-3
Molecular Formula:C₂₃H₂₉N₇O₃*ClH
Molecular Weight:487.989
Hs Code.:

Synonyms:(1r,4r)-4-((4-(2H-indazol-4-yl)-6-morpholino-1,3,5-triazine-2-yl)oxy)-N,N-dimethycyclohexanecarboxamide hydrochloride

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Chemical Property of (1r,4r)-4-((4-(2H-indazol-4-yl)-6-morpholino-1,3,5-triazine-2-yl)oxy)-N,N-dimethycyclohexanecarboxamide hydrochloride

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Technology Process of (1r,4r)-4-((4-(2H-indazol-4-yl)-6-morpholino-1,3,5-triazine-2-yl)oxy)-N,N-dimethycyclohexanecarboxamide hydrochloride

There total 10 articles about (1r,4r)-4-((4-(2H-indazol-4-yl)-6-morpholino-1,3,5-triazine-2-yl)oxy)-N,N-dimethycyclohexanecarboxamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1542268-07-4
C₂₈H₃₇N₇O₄

: 1542268-06-3
(1r,4r)-4-((4-(2H-indazol-4-yl)-6-morpholino-1,3,5-triazine-2-yl)oxy)-N,N-dimethycyclohexanecarboxamide hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 24h;

Reference yield:

: 1391926-33-2
4-(4-(benzylthio)-6-chloro-1,3,5-triazin-2-yl)morpholine

: 1542268-06-3
(1r,4r)-4-((4-(2H-indazol-4-yl)-6-morpholino-1,3,5-triazine-2-yl)oxy)-N,N-dimethycyclohexanecarboxamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 90 °C / Inert atmosphere

2: Oxone / tetrahydrofuran; water / 25 h / 0 - 20 °C

3: sodium hydride / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

4: hydrogenchloride / 1,4-dioxane / 24 h / 20 °C

With hydrogenchloride; Oxone; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; sodium carbonate; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water;

Reference yield:

: 1391926-34-3
4-(4-(benzylthio)-6-(2-(tetrahydro-2H-pyran-2-yl)-2H-indazol-4-yl)-1,3,5-triazin-2-yl)morpholine

: 1542268-06-3
(1r,4r)-4-((4-(2H-indazol-4-yl)-6-morpholino-1,3,5-triazine-2-yl)oxy)-N,N-dimethycyclohexanecarboxamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: Oxone / tetrahydrofuran; water / 25 h / 0 - 20 °C

2: sodium hydride / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

3: hydrogenchloride / 1,4-dioxane / 24 h / 20 °C

With hydrogenchloride; Oxone; sodium hydride; In tetrahydrofuran; 1,4-dioxane; water;