(R)-2-amino-5-[4-(tert-butyl-dimethylsilanyloxy)phenyl]-pentanoic acid amide

Base Information

• Chemical Name: (R)-2-amino-5-[4-(tert-butyl-dimethylsilanyloxy)phenyl]-pentanoic acid amide
• CAS No.: 1160754-94-8
• Molecular Formula: C₁₇H₃₀N₂O₂Si
• Molecular Weight: 322.523

Synonyms:(R)-2-amino-5-[4-(tert-butyl-dimethylsilanyloxy)phenyl]-pentanoic acid amide

Chemical Property of (R)-2-amino-5-[4-(tert-butyl-dimethylsilanyloxy)phenyl]-pentanoic acid amide

Chemical Property:

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Technology Process of (R)-2-amino-5-[4-(tert-butyl-dimethylsilanyloxy)phenyl]-pentanoic acid amide

There total 5 articles about (R)-2-amino-5-[4-(tert-butyl-dimethylsilanyloxy)phenyl]-pentanoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-2-amino-5-(4-hydroxyphenyl)pentanoic acid amide hydrochloride + tert-butyldimethylsilyl chloride (18162-48-6) → (R)-2-amino-5-[4-(tert-butyl-dimethylsilanyloxy)phenyl]-pentanoic acid amide (1160754-94-8)

Guidance literature:

With 1H-imidazole; In tetrahydrofuran; at 70 ℃; for 4h;

Reference yield:

(R)-2-amino-5-(4-hydroxyphenyl)pentanoic acid amide (1160754-93-7) + tert-butyldimethylsilyl chloride (18162-48-6) → (R)-2-amino-5-[4-(tert-butyl-dimethylsilanyloxy)phenyl]-pentanoic acid amide (1160754-94-8)

Guidance literature:

With 1H-imidazole; In tetrahydrofuran; at 70 ℃; for 4h;

Reference yield:

1H-imidazole (288-32-4) + (R)-2-amino-5-(4-hydroxyphenyl)pentanoic acid amide (1160754-93-7) + tert-butyldimethylsilyl chloride (18162-48-6) → (R)-2-amino-5-[4-(tert-butyl-dimethylsilanyloxy)phenyl]-pentanoic acid amide (1160754-94-8)

Guidance literature:

In tetrahydrofuran; diethyl ether;

upstream raw materials:

1H-imidazole

(R)-2-amino-5-(4-hydroxyphenyl)pentanoic acid amide

tert-butyldimethylsilyl chloride

[(R)-4-(4-tert-butoxyphenyl)-1-carbamoyl-butyl]-carbamic acid tert-butyl ester

Downstream raw materials:

4-((R)-4,5-diaminopentyl)phenol

3,5-diamino-6-chloro-pyrazine-2-carboxylic acid [(R)-4-[3-(4-hydroxyphenyl)-propyl]imidazolidin-(2E)-ylidene]amide

3,5-diamino-6-chloropyrazine-2-carboxylic acid [(R)-4-{3-[4-((S)-2,3-dihydroxypropoxy)phenyl]propyl}imidazolidin-(2Z)-ylidene]amide

(R)-3-[4-((R)-4,5-diaminopentyl)phenoxy]-propane-1,2-diol

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