4-nitrobenzyl nicotinate

Base Information

Chemical Name:4-nitrobenzyl nicotinate
CAS No.:4457-25-4
Molecular Formula:C₁₃H₁₀N₂O₄
Molecular Weight:258.233
Hs Code.:

Synonyms:4-nitrobenzyl nicotinate

Suppliers and Price of 4-nitrobenzyl nicotinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-nitrobenzyl nicotinate

Chemical Property:

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Technology Process of 4-nitrobenzyl nicotinate

There total 2 articles about 4-nitrobenzyl nicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 59-67-6
nicotinic acid

: 99-99-0
1-methyl-4-nitrobenzene

: 4457-25-4
4-nitrobenzyl nicotinate

Guidance literature:: 1-methyl-4-nitrobenzene; With tert.-butylhydroperoxide; N-Bromosuccinimide; In neat (no solvent); at 80 ℃; for 2h;

nicotinic acid; With triethylamine; In neat (no solvent); at 80 ℃; for 1h;
DOI:10.1016/j.tet.2014.04.041

Reference yield:

: 59-67-6
nicotinic acid

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 4457-25-4
4-nitrobenzyl nicotinate

Guidance literature:: With caesium carbonate; Yield given; 1.) H₂O, room temperature, 2.) DMF, room tempereature, overnight;
DOI:10.1135/cccc19942057