2-Acetylamino-6,6-dimethoxy-5-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

Base Information

Chemical Name:2-Acetylamino-6,6-dimethoxy-5-(toluene-4-sulfonylamino)-hexanoic acid methyl ester
CAS No.:124920-23-6
Molecular Formula:C₁₈H₂₈N₂O₇S
Molecular Weight:416.496
Hs Code.:

Synonyms:2-Acetylamino-6,6-dimethoxy-5-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

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Chemical Property of 2-Acetylamino-6,6-dimethoxy-5-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

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Technology Process of 2-Acetylamino-6,6-dimethoxy-5-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

There total 2 articles about 2-Acetylamino-6,6-dimethoxy-5-(toluene-4-sulfonylamino)-hexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 67-56-1
methanol

: 124920-22-5
α-N-acetyl-ε-N-tosyl-L-lysine methyl ester

: 124920-23-6
2-Acetylamino-6,6-dimethoxy-5-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

Guidance literature:: With sodium methylate; potassium iodide; 1.) anodic oxidation, -10 deg C, 2.) anodic oxidation, 25 deg C;

Reference yield:

: 94251-50-0
α-N-acetyl-ε-N-tosyl-L-lysine

: 124920-23-6
2-Acetylamino-6,6-dimethoxy-5-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / HCl (gas)

2: 92 percent / KI, NaOMe / 1.) anodic oxidation, -10 deg C, 2.) anodic oxidation, 25 deg C

With hydrogenchloride; sodium methylate; potassium iodide;

Reference yield:

: 124920-23-6
2-Acetylamino-6,6-dimethoxy-5-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

: 124920-25-8
(2R,5R)-1-Acetyl-5-(toluene-4-sulfonylamino)-piperidine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / NH₄Cl / 3 h / 130 °C / 20 Torr

2: 78 percent / H₂ / PtO₂ / acetic acid / 7600 Torr

With hydrogen; ammonium chloride; platinum(IV) oxide; In acetic acid;