Malonic acid 3-hydroxy-5-(2-octadecyloxycarbonyl-acetoxymethyl)-benzyl ester octadecyl ester

Base Information

Chemical Name:Malonic acid 3-hydroxy-5-(2-octadecyloxycarbonyl-acetoxymethyl)-benzyl ester octadecyl ester
CAS No.:868051-65-4
Molecular Formula:C₅₀H₈₆O₉
Molecular Weight:831.227
Hs Code.:

Synonyms:Malonic acid 3-hydroxy-5-(2-octadecyloxycarbonyl-acetoxymethyl)-benzyl ester octadecyl ester

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Chemical Property of Malonic acid 3-hydroxy-5-(2-octadecyloxycarbonyl-acetoxymethyl)-benzyl ester octadecyl ester

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Technology Process of Malonic acid 3-hydroxy-5-(2-octadecyloxycarbonyl-acetoxymethyl)-benzyl ester octadecyl ester

There total 4 articles about Malonic acid 3-hydroxy-5-(2-octadecyloxycarbonyl-acetoxymethyl)-benzyl ester octadecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1002-31-9
2-((octadecyloxy)carbonyl)acetic acid

: 153707-56-3
3,5-bis(hydroxymethyl)phenol

: 868051-65-4
Malonic acid 3-hydroxy-5-(2-octadecyloxycarbonyl-acetoxymethyl)-benzyl ester octadecyl ester

Guidance literature:: With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/ejic.200600875

Reference yield:

: 112-92-5
1-octadecanol

: 868051-65-4
Malonic acid 3-hydroxy-5-(2-octadecyloxycarbonyl-acetoxymethyl)-benzyl ester octadecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 1 h / 110 - 120 °C

2: 53 percent / N,N'-dicyclohexylcarbodiimide; DMAP; HOBT / tetrahydrofuran / 3 h

With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2005.08.038

Reference yield:

: 618-83-7
5-Hydroxyisophthalic acid

: 868051-65-4
Malonic acid 3-hydroxy-5-(2-octadecyloxycarbonyl-acetoxymethyl)-benzyl ester octadecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / H₂SO₄ / 24 h / Heating

2: 85 percent / LAH / tetrahydrofuran / 24 h / Heating

3: 53 percent / N,N'-dicyclohexylcarbodiimide; DMAP; HOBT / tetrahydrofuran / 3 h

With dmap; lithium aluminium tetrahydride; sulfuric acid; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2005.08.038