C₆H₅N(CH₃)2H⁽¹⁺⁾*B(C₆F₄C(C₆F₅)2F)4^(1-)=C₆H₅N(CH₃)2HB(C₆F₄C(C₆F₅)2F)4

Base Information

• Chemical Name: C₆H₅N(CH₃)2H⁽¹⁺⁾*B(C₆F₄C(C₆F₅)2F)4^(1-)=C₆H₅N(CH₃)2HB(C₆F₄C(C₆F₅)2F)4
• CAS No.: 346722-58-5
• Molecular Formula: C₈H₁₁N*C₇₆BF₆₀*H
• Molecular Weight: 2185.74
• Mol file: 346722-58-5.mol

Synonyms:C₆H₅N(CH₃)2H⁽¹⁺⁾*B(C₆F₄C(C₆F₅)2F)4^(1-)=C₆H₅N(CH₃)2HB(C₆F₄C(C₆F₅)2F)4

Chemical Property of C₆H₅N(CH₃)2H⁽¹⁺⁾*B(C₆F₄C(C₆F₅)2F)4^(1-)=C₆H₅N(CH₃)2HB(C₆F₄C(C₆F₅)2F)4

Chemical Property:

Purity/Quality:

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Technology Process of C₆H₅N(CH₃)2H⁽¹⁺⁾*B(C₆F₄C(C₆F₅)2F)4^(1-)=C₆H₅N(CH₃)2HB(C₆F₄C(C₆F₅)2F)4

There total 1 articles about C₆H₅N(CH₃)2H⁽¹⁺⁾*B(C₆F₄C(C₆F₅)2F)4^(1-)=C₆H₅N(CH₃)2HB(C₆F₄C(C₆F₅)2F)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

HC6F4C(C6F5)2F (346722-56-3) + boron trichloride (10294-34-5) + N,N-dimethylaniline hydrochloride (5882-44-0) → C6H5N(CH3)2H(1+)*B(C6F4C(C6F5)2F)4(1-)=C6H5N(CH3)2HB(C6F4C(C6F5)2F)4 (346722-58-5)

Guidance literature:

With n-butyllithium; In diethyl ether; hexane; byproducts: LiCl; a soln. perfluoro-compound in diethyl ether was treated at -78°C with n-BuLi, stirred for 45 min, BCl3 in hexane was added, stirred for 20 min, warmed and stirred for 1 h, a soln. of amine in CH2Cl2 was added,stirred for 1 h (inert atm.); LiCl was filtered off, the solvent was evapd., treated with pentane;

DOI:10.1021/om001080i

upstream raw materials:

HC₆F₄C(C₆F₅)2F

boron trichloride

N,N-dimethylaniline hydrochloride